Microwave-Assisted Solvothermal Synthesis and Characterization of Barium Orthovanadate Nanoparticles

被引：6
作者：
Lim, Chang Sung [1 ]
机构：
[1] Hanseo Univ, Dept Adv Mat Sci & Engn, Seosan 356706, South Korea
来源：
ASIAN JOURNAL OF CHEMISTRY | 2013年 / 25卷 / 05期
基金：
新加坡国家研究基金会;
关键词：
Barium orthovanadate; Microwave-assited solvothermal synthesis; Nanoparticles; Luminescence; Raman spectroscopy; KAGOME-STAIRCASE LATTICE; M3V2O8; M; CRYSTALS; RADIATION; CO3V2O8; CAMOO4; STATE; ZN;
D O I：
10.14233/ajchem.2013.CSLimA
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Barium-orthovanadate (Ba3V2O8) nanoparticles were synthesized successfully using a facile microwave solvothermal route followed by further heat-treatment. Well-crystallized Ba3V2O8 nanoparticles warp formed after heat-treatment at 600 degrees C for 3 h showing a fine and homogeneous morphology with particle sizes of 50-150 nm. The synthesized Ba3V2O8 nanoparticles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. The optical properties were investigated by photoluminescence emission and Raman spectroscopy.
引用
收藏
页码：2395 / 2398
页数：4
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