Influence of Spark Plasma Sintering Temperature on the Densification, Microstructure and Mechanical Properties of Al-4.5 wt.%Cu Alloy

被引:21
作者
Devaraj, S. [1 ]
Sankaran, S. [1 ]
Kumar, R. [1 ]
机构
[1] Indian Inst Technol, Dept Met & Mat Engn, Madras 600036, Tamil Nadu, India
关键词
Spark plasma sintering; Sintering mechanisms; Precipitation; Compression strength; METAL-MATRIX COMPOSITES; AL; PARAMETERS;
D O I
10.1007/s40195-013-0159-z
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
The effect of sintering temperature on the densification mechanisms, microstructural evolution and mechanical properties of spark plasma sintered (SPS) compacts of a gas atomized Al-4.5 wt.%Cu alloy was investigated. The powder particles whose size varied between 10 to 500 mu m was subjected to SPS at 400, 450 and 500 degrees C at a pressure of 30 MPa. The compact sintered at 500 degrees C exhibited fully dense microstructure which was characterized by a uniform distribution of the secondary phase, free of dendrites and micro-porosity. Microscopy and the SPS data reveal that the events such as particle rearrangement, localized deformation and bulk deformation appear to be the sequence of sintering mechanisms depending on the size range of powder particles used for consolidation. The compact sintered at 500 degrees C exhibited the highest hardness and compression strength since the microstructure was characterized by fine distribution of precipitates, large fraction of sub-micron grains and complete metallurgical bonding.
引用
收藏
页码:761 / 771
页数:11
相关论文
共 36 条
[1]  
Abe Y., 1998, MATER SCI ENG, V98, P351
[2]   Local modifications of magnetism and structure in FePt (001) epitaxial thin films by focused ion beam: Two-dimensional perpendicular patterns [J].
Albertini, F. ;
Nasi, L. ;
Casoli, F. ;
Fabbrici, S. ;
Luches, P. ;
Gazzadi, G. C. ;
di Bona, A. ;
Vavassori, P. ;
Valeri, S. ;
Contri, S. F. .
JOURNAL OF APPLIED PHYSICS, 2008, 104 (05)
[3]   Microcasting of Al bronze:: influence of casting parameters on the microstructure and the mechanical properties [J].
Baumeister, Gundi ;
Okolo, Brando ;
Roegner, Joachim .
MICROSYSTEM TECHNOLOGIES-MICRO-AND NANOSYSTEMS-INFORMATION STORAGE AND PROCESSING SYSTEMS, 2008, 14 (9-11) :1647-1655
[4]  
BRODY HD, 1966, T METALL SOC AIME, V236, P615
[5]   Densification mechanisms in spark plasma sintering of nanocrystalline ceramics [J].
Chaim, Rachman .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2007, 443 (1-2) :25-32
[6]   Densification mechanisms in spark plasma sintering: Effect of particle size and pressure [J].
Diouf, S. ;
Molinari, A. .
POWDER TECHNOLOGY, 2012, 221 :220-227
[7]  
Fleury E., 2001, MAT RES SOC S, V643
[8]   Current effects on neck growth in the sintering of copper spheres to copper plates by the pulsed electric current method [J].
Frei, James M. ;
Anselmi-Tamburini, Umberto ;
Munir, Zuhair A. .
JOURNAL OF APPLIED PHYSICS, 2007, 101 (11)
[9]   VACANCIES AND PRECIPITATES IN AL-1.9 AT-PERCENT CU STUDIED BY POSITRONS [J].
GLASER, UH ;
DLUBEK, G ;
KRAUSE, R .
PHYSICA STATUS SOLIDI B-BASIC RESEARCH, 1991, 163 (02) :337-343
[10]   Sintering activation by external electrical field [J].
Groza, JR ;
Zavaliangos, A .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2000, 287 (02) :171-177