Synthesis and characterization of poly (Itaconic Acid-m-Phen-ylenediamine)

被引：0

作者：

Wang, Chuanxing ^{[1
]}

Wang, Pengfei ^{[1
]}

Xu, Qinhong ^{[1
]}

Wei, Zhe ^{[1
]}

Wu, Yumin ^{[1
]}

机构：

[1] Qingdao Univ Sci & Technol, Coll Chem Engn, Qingdao 266042, Peoples R China

来源：

PROCEEDINGS OF THE 2016 INTERNATIONAL CONFERENCE ON INNOVATIVE MATERIAL SCIENCE AND TECHNOLOGY (IMST 2016) | 2016年 / 139卷

关键词：

low temperature solution polycondensation; itaconyl chloride; polymer; inherent viscosity; characterization;

D O I：

暂无

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

With Itaconyl chloride and m-phenylenediamine as raw materials, poly(itaconic acid-m-phenylenediamine) was synthesized by the low temperature solution polycondensation we reported. The effects of initial temperature and reaction time on polycondensation were investigated. And the product was characterized by H-1-NMR, FT-IR and TGA. The results showed that the polycondensation should carry out at a low temperature. The initial temperature should be lower 0 degrees C. The polycondensation time was 90-100 minutes. Under these conditions, the thermal stability was good and its inherent viscosity was about 1.4. The spectra of FT-IR and 1H-NMR confirmed its structure.

引用

页码：18 / 24

页数：7

共 12 条

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