Application of Fourier Transform Near-Infrared Spectroscopy Combined with High-Performance Liquid Chromatography in Rapid and Simultaneous Determination of Essential Components in Crude Radix Scrophulariae

被引：5
|
作者：
Li, Xiaomeng [1 ]
Fang, Dansi
Cong, Xiaodong [1 ]
Cao, Gang [1 ,3 ]
Cai, Hao [2 ,3 ]
Cai, Baochang [1 ,2 ,3 ]
机构：
[1] Zhejiang Chinese Med Univ, Res Ctr TCM Proc Technol, Hangzhou, Zhejiang, Peoples R China
[2] Nanjing Univ Chinese Med, Engn Ctr State Minist Educ Standardizat Chinese M, Nanjing, Jiangsu, Peoples R China
[3] Nanjing Univ Chinese Med, Natl Class Key Discipline Tradit Chinese Med 1, Nanjing, Jiangsu, Peoples R China
来源：
AAPS PHARMSCITECH | 2012年 / 13卷 / 04期
基金：
中国国家自然科学基金;
关键词：
crude Radix Scrophulariae; FT-NIRS; HPLC-DAD; quality control; quantification; QUALITY-CONTROL; QUANTIFICATION; HPLC; DISCRIMINATION; CONSTITUENTS; EXTRACT; NIRS;
D O I：
10.1208/s12249-012-9867-3
中图分类号：
R9 [药学];
学科分类号：
1007 ;
摘要：
A method is described using rapid and sensitive Fourier transform near-infrared spectroscopy combined with high-performance liquid chromatography-diode array detection for the simultaneous identification and determination of four bioactive compounds in crude Radix Scrophulariae samples. Partial least squares regression is selected as the analysis type and multiplicative scatter correction, second derivative, and Savitzky-Golay filter were adopted for the spectral pretreatment. The correlation coefficients (R) of the calibration models were above 0.96 and the root mean square error of predictions were under 0.028. The developed models were applied to unknown samples with satisfactory results. The established method was validated and can be applied to the intrinsic quality control of crude Radix Scrophulariae.
引用
收藏
页码：1428 / 1435
页数：8
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