Synthesis and spectroscopic characterization of some divalent metal complexes derived from 1,4-dibenzoylthiosemicarbazide and N-[2-(3-benzoylthioureido)ethyl]benzamide

被引：3

作者：

Ahmed, IT ^{[1
]}

机构：

[1] ElMinia Univ, Dept Chem, Fac Sci, Menia 61519, Egypt

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2006年 / 181卷 / 02期

关键词：

1,4-dibenzoylthiosemicarbazide; binary metal complexes; N-[2-(3-benzoylthioureido)ethyl]benzamide;

D O I：

10.1080/104265090970296

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The binary metal complexes [M(II)-L-1 or L-2], where M(II) = Co(II), Ni(II), Cu(II), Zn(II), Pb(II), Cd(II) and UO2(II); L-1 = 1,4-dibenzoylthiosemicarbazide; and L-2 = N-[2-(3-benzoylthioureido)ethyl]benzamide; were prepared and characterized by elemental analysis, thermogravimetric analysis, molar conductance, and electronic spectro-scopies (IR, H-1-, and C-13-NMR) in addition to mass spectra.

引用

页码：267 / 278

页数：12

共 37 条

[21] Bisthiosemicarbazones of 2,4-pentanedione are pyrazolines [J].

Hunter, DH ;

McRoberts, C ;

Vittal, JJ .

CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1998, 76 (05) :522-524

[22] STRUCTURAL STUDIES OF 1-ISATIN-4-PHENYL-3-THIOSEMICARBAZONE AND 1-(ALPHA-)FURYL-4-PHENYL-3-THIOSEMICARBAZONE COMPLEXES [J].

IBRAHIM, KM ;

ELASMY, AA ;

BEKHEIT, MM ;

MOSTAFA, MM .

SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY, 1985, 15 (09) :1247-1259

[23]

KAIM W, 1994, BIOORGANIC CHEM INOR, P371

[24]

Labisbal E, 2002, Z NATURFORSCH B, V57, P908

[25] SYNTHESIS OF 5,6-DIHYDRO-8(7H)-QUINOLINONE THIOSEMICARBAZONES AS POTENTIAL ANTITUMOR AGENTS [J].

LEMKE, TL ;

SHEK, TW ;

CATES, LA ;

SMITH, LK ;

COSBY, LA ;

SARTORELLI, AC .

JOURNAL OF MEDICINAL CHEMISTRY, 1977, 20 (10) :1351-1354

[26] Rhenium(V) oxo complexes of novel N2S2 dithiourea (DTU) chelate ligands: Synthesis and structural characterization [J].

Lipowska, M ;

Hayes, BL ;

Hansen, L ;

Taylor, A ;

Marzilli, LG .

INORGANIC CHEMISTRY, 1996, 35 (14) :4227-4231

[27]

Mekuskiene G, 2002, J CHEM RES, P213

[28]

Mel'nyk OP, 2001, Z ANORG ALLG CHEM, V627, P287, DOI 10.1002/1521-3749(200102)627:2<287::AID-ZAAC287>3.0.CO

[29]

2-P

[30]

Nakamoto K., 1978, INFRARED RAMAN SPECT

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