Process parameters in the manufacture of ceramic ZnO nanofibers made by electrospinning

被引:5
|
作者
Nonato, Renato C. [1 ]
Morales, Ana R. [1 ]
Rocha, Mateus C. [1 ]
Nista, Silvia V. G. [1 ]
Mei, Lucia H. I. [1 ]
Bonse, Baltus C. [2 ]
机构
[1] Univ Campinas Unicamp, DEMBIO, Campinas, SP, Brazil
[2] Ctr Univ FEI, Sao Bernardo Do Campo, SP, Brazil
来源
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2017年 / 123卷 / 01期
关键词
POLYETHYLENE FIBERS; ACID-SOLUTION; THIN-FILMS; MATS; NANOCOMPOSITES; MORPHOLOGY;
D O I
10.1007/s00339-016-0717-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Zinc oxide (ZnO) nanofibers were prepared by electrospinning under different conditions using a solution of poly(vinyl alcohol) and zinc acetate as precursor. A 2(3) factorial design was made to study the influence of the process parameters in the electrospinning (collector distance, flow rate and voltage), and a 2(2) factorial design was made to study the influence of the calcination process (time and temperature). SEM images were made to analyze the fiber morphology before and after calcination process, and the images were made to measure the nanofiber diameter. X-ray diffraction was made to analyze the total precursor conversion to ZnO and the elimination of the polymeric carrier.
引用
收藏
页数:8
相关论文
共 50 条
  • [11] Electrospinning process parameters optimization for biofunctional curcumin/gelatin nanofibers
    Kanu, Nand Jee
    Gupta, Eva
    Vales, Umesh Kumar
    Singh, Gyanendra Kumar
    MATERIALS RESEARCH EXPRESS, 2020, 7 (03)
  • [13] Affecting parameters on electrospinning process and characterization of electrospun gelatin nanofibers
    Okutan, Nagihan
    Terzi, Pinar
    Altay, Filiz
    FOOD HYDROCOLLOIDS, 2014, 39 : 19 - 26
  • [14] Ceramic nanofibers by electrospinning technique - A review
    Panda, P. K.
    TRANSACTIONS OF THE INDIAN CERAMIC SOCIETY, 2008, 66 (02) : 65 - 76
  • [15] Fabrication and characterization of ZnO nanofibers by electrospinning
    Park, Jin-Ah
    Moon, Jaehyun
    Lee, Su-Jae
    Lim, Sang-Chul
    Zyung, Taehyoung
    CURRENT APPLIED PHYSICS, 2009, 9 : S210 - S212
  • [16] Preparation and characterization of ZnO nanofibers by electrospinning
    Siddheswaran, R.
    Sankar, R.
    Babu, M. Ramesh
    Rathnakumari, M.
    Jayavel, R.
    Murugakoothan, P.
    Sureshkumar, P.
    CRYSTAL RESEARCH AND TECHNOLOGY, 2006, 41 (05) : 446 - 449
  • [17] Composite pullulan-whey protein nanofibers made by electrospinning: Impact of process parameters on fiber morphology and physical properties
    Drosou, Christina
    Krokida, Magdalini
    Biliaderis, Costas G.
    FOOD HYDROCOLLOIDS, 2018, 77 : 726 - 735
  • [18] Electrospinning process parameters dependent investigation of TiO2 nanofibers
    Someswararao, M. V.
    Dubey, R. S.
    Subbarao, P. S. V.
    Singh, Shyam
    RESULTS IN PHYSICS, 2018, 11 : 223 - 231
  • [19] Manufacture and Characterization of Poly (butylene terephthalate) Nanofibers by Electrospinning
    Forouharshad, Mehdi
    Saligheh, Omid
    Arasteh, Rouhollah
    Farsani, Reza Eslami
    JOURNAL OF MACROMOLECULAR SCIENCE PART B-PHYSICS, 2010, 49 (04): : 833 - 842
  • [20] Fabrication of ceramic and composite nanofibers by electrospinning.
    Li, D
    Xia, YN
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2003, 226 : U425 - U425