A convenient synthesis of N-substituted 2-thioxo-1,3-thiazolidin-4-ones

被引：17

作者：

Yarovenko, VN

Nikitina, AS

Zavarzin, IV

Krayushkin, MM

Kovalenko, LV

机构：

[1] Russian Acad Sci, ND Zelinskii Organ Chem Inst, Moscow 119991, Russia

[2] DI Mendeleev Russian Univ Chem Technol, Moscow 125047, Russia

来源：

SYNTHESIS-STUTTGART | 2006年 / 8卷 / 08期

关键词：

oxamic acid thiohydrazides; amines; hydrazides; rhodanines; carbodiimide; 1,1 '-carbonyldiimidazole;

D O I：

10.1055/s-2006-926409

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A convenient method was developed for the synthesis of N-substituted rhodanines based on the reaction of amines, hydrazides, or acid thiohydrazides with trithiocarbonyl di.glycolic acid in the presence of dicyclohexylcarbodiimide or 1,1'-carbonyldiimidazole.

引用

页码：1246 / 1248

页数：3

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[2]

JOHANNES SB, 1931, J AM CHEM SOC, V53, P2688

[3]

KLINE S, 1973, Patent No. 2325038

[4] Synthesis and reactivity of monothiooxamides and thiohydrazides of oxamic acids [J].