Separation of the cyclopeptide heterophyllin B by high-speed countercurrent chromatography and its application as a new stationary phase for capillary gas chromatography

被引：13
作者：
Yuan, LM [1 ]
Fu, RN
Tan, NH
Ai, P
Zhou, J
Wu, P
Zi, M
机构：
[1] Yunnan Normal Univ, Dept Chem, Kunming 650092, Peoples R China
[2] Beijing Inst Technol, Dept Chem, Beijing 100081, Peoples R China
[3] Acad Sinica, Lab Phytochem, Kunming Inst Bot, Kunming 650204, Peoples R China
来源：
ANALYTICAL LETTERS | 2002年 / 35卷 / 01期
基金：
中国国家自然科学基金;
关键词：
capillary gas chromatography; high-speed countercurrent chromatography stationary phase; cyclopeptide heterophyllin B;
D O I：
10.1081/AL-120002372
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
From the root of Pseudostellaria heterophylla a cyclopeptide, heterophyllin B, was isolated by high-speed countercurrent chromatography. Fused-silica capillary columns containing heterophyllin B as a main stationary phase component were prepared. The chromatographic selectivity of heterophyllin B showed toward aromatics. electron attracting compounds and amino acid.
引用
收藏
页码：203 / 212
页数：10
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