Household processing factors of acrinathrin, fipronil, kresoxim-methyl and pyridaben residues in green beans

被引:43
作者
Aguilera, Ana [1 ]
Valverde, Antonio [1 ]
Camacho, Francisco [2 ]
Boulaid, Mourad [1 ]
Garcia-Fuentes, Luis [3 ]
机构
[1] Univ Almeria, Pesticide Residue Res Grp, Fac Expt Sci, Almeria 04120, Spain
[2] Univ Almeria, Vegetal Prod Dept, Fac Agron, Almeria 04120, Spain
[3] Univ Almeria, Chem & Phys Dept, Fac Expt Sci, Almeria 04120, Spain
关键词
Pyridaben; Acrinathrin; Kresoxim-methyl; Fipronil; Green beans; Household processing; PESTICIDE-RESIDUES; LIQUID-CHROMATOGRAPHY; UNIT VARIABILITY; VEGETABLES; FRUITS; TRALOMETHRIN; VALIDATION; PRODUCTS; TOMATOES; RISK;
D O I
10.1016/j.foodcont.2013.06.038
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
The influence of household washing and boiling processes on the residue levels of acrinathrin, fipronil, kresoxim-methyl and pyridaben in green beans was studied. The study was conducted on green beans samples collected from an experimental greenhouse during a two weeks period after treatment. Analyses were carried out by QuEChERS extraction method and gas chromatography with electron-capture detection (GC/ECD). Pesticide levels in the unprocessed green beans samples where within the range of 0.1 and 4 mg/kg. The washing processing factors were 0.51 for fipronil, 0.32 for pyridaben, 0.59 for acrinathrin and 038 for kresoxim-methyl whereas the boiling factor ranged between 0.50 and 0.72. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:146 / 152
页数:7
相关论文
共 29 条
[21]  
Lehotay SJ, 2005, J AOAC INT, V88, P615
[22]   Benefits and pitfalls of the application of screening methods for the analysis of pesticide residues in fruits and vegetables [J].
Malato, Octavio ;
Lozano, Ana ;
Mezcua, Milagros ;
Agueera, Ana ;
Fernandez-Alba, Amadeo R. .
JOURNAL OF CHROMATOGRAPHY A, 2011, 1218 (42) :7615-7626
[24]   Total diet study on pesticide residues in France: Levels in food as consumed and chronic dietary risk to consumers [J].
Nougadere, Alexandre ;
Sirot, Veronique ;
Kadar, Ali ;
Fastier, Antony ;
Truchot, Eric ;
Vergnet, Claude ;
Hommet, Frederic ;
Bayle, Joelle ;
Gros, Philippe ;
Leblanc, Jean-Charles .
ENVIRONMENT INTERNATIONAL, 2012, 45 :135-150
[25]   Analytical methods for estimation of organophosphorus pesticide residues in fruits and vegetables: A review [J].
Sharma, Dipakshi ;
Nagpal, Avinash ;
Pakade, Yogesh B. ;
Katnoria, Jatinder Kaur .
TALANTA, 2010, 82 (04) :1077-1089
[26]  
STREET JC, 1969, CAN MED ASSOC J, V100, P154
[27]  
Tomlin C.D.S., 2009, PESTICIDE MANUAL
[28]   Pesticide residue levels in peppers grown in a greenhouse after multiple applications of pyridaben and tralomethrin [J].
Valverde, A ;
Aguilera, A ;
Rodríguez, M ;
Boulaid, M ;
Soussu-El Begrani, M .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2002, 50 (25) :7303-7307
[29]   Analysis of Forchlorfenuron in Vegetables by LC/TOF-MS after Extraction with the Buffered QuEChERS Method [J].
Valverde, Antonio ;
Aguilera, Ana ;
Ferrar, Carmen ;
Camacho, Francisco ;
Cammarano, Anita .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2010, 58 (05) :2818-2823