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Ethylene glycol assisted hydrothermal synthesis of strontium hexaferrite nanoparticles as precursor of magnetic fluid
被引:34
作者:
Tang, X.
[1
,2
]
Hong, R. Y.
[1
,2
,3
]
Feng, W. G.
[4
]
Badami, D.
[5
]
机构:
[1] Soochow Univ, SIP, Coll Chem Chem Engn & Mat Sci, Suzhou 215123, Peoples R China
[2] Soochow Univ, SIP, Key Lab Organ Synth Jiangsu Prov, Suzhou 215123, Peoples R China
[3] Fuzhou Univ, Coll Chem & Chem Engn, Fuzhou 350002, Peoples R China
[4] Suzhou Nanocomp Inc, Suzhou 215011, Peoples R China
[5] Univ Waterloo, Dept Chem Engn, Waterloo, ON N2L 3G1, Canada
基金:
中国国家自然科学基金;
关键词:
Strontium hexaferrite;
Hydrothermal synthesis;
Magnetic fluid;
Hyperthermia;
FE3O4;
NANOPARTICLES;
HYPERTHERMIA;
FERROFLUIDS;
POWDERS;
COMBUSTION;
PARTICLES;
FERRITE;
DESIGN;
WATER;
D O I:
10.1016/j.jallcom.2013.02.049
中图分类号:
O64 [物理化学(理论化学)、化学物理学];
学科分类号:
070304 ;
081704 ;
摘要:
Strontium hexaferrite (SrFe12O19) nanoparticles were prepared using ethylene glycol (EG) assisted hydrothermal synthesis. The experimental results revealed that the reaction temperature and the amount of EG had an effect on the size, morphology and magnetic properties of SrFe12O19 nanoparticles. SrFe12O19 nanoparticles with a size of about 25 nm were obtained at 140 degrees C for 24 h at the EG/W volumetric ratios of 1/1. The saturation magnetization of the particles was approximately 10.6 emu/g. Furthermore, SrFe12O19 nanoparticles modified by oleic acid could be dispersed in high boiling point mineral oil to form highly-concentrated magnetic fluid. The magnetic and rheological properties of magnetic fluid were investigated using a Gouy magnetic balance and a rotational rheometer, respectively. The magnetic fluid showed excellent stability in gravity field and external magnetic field, and exhibited shear-thinning behavior. Moreover, the magnetic fluid had obvious heating effect in an alternating magnetic field and had potential on hyperthermia therapy of tumor. (C) 2013 Elsevier B. V. All rights reserved.
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页码:211 / 218
页数:8
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