Synthesis of titanium-oxide nanoparticles with size and stoichiometry control

被引:15
作者
Gunnarsson, Rickard [1 ]
Helmersson, Ulf [1 ]
Pilch, Iris [2 ]
机构
[1] Linkoping Univ, Plasma & Coatings Phys Div, IFM Mat Sci, S-58183 Linkoping, Sweden
[2] Linkoping Univ, Thin Film Phys Div, IFM Mat Sci, S-58183 Linkoping, Sweden
基金
瑞典研究理事会;
关键词
Titanium dioxide; TiO2; Reactive sputtering; Size control; Composition control; Gas flow sputtering; Aerosols; REACTIVE SPUTTERING PROCESSES; MAGNETRON; DEPOSITION; FILMS;
D O I
10.1007/s11051-015-3158-3
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Ti-O nanoparticles have been synthesized via hollow cathode sputtering in an Ar-O-2 atmosphere using high power pulsing. It is shown that the stoichiometry and the size of the nanoparticles can be varied independently, the former through controlling the O-2 gas flow and the latter by the independent biasing of two separate anodes in the growth zone. Nanoparticles with diameters in the range of 25-75 nm, and with different Ti-O compositions and crystalline phases, have been synthesized.
引用
收藏
页数:11
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