Application of Laser-Backscattering Instruments for In Situ Monitoring of Crystallization Processes - A Review

被引：49

作者：

Heinrich, Joerg ^{[1
]}

Ulrich, Joachim ^{[1
]}

机构：

[1] Univ Halle Wittenberg, Ctr Engn Thermal Proc Technol, D-06120 Halle, Saale, Germany

来源：

CHEMICAL ENGINEERING & TECHNOLOGY | 2012年 / 35卷 / 06期

关键词：

Chord length distribution; Crystallization; Focused beam reflectance measurement; Particle size analysis; Threefold dynamical optical reflectance measurement; BEAM REFLECTANCE MEASUREMENT; PARTICLE-SIZE DISTRIBUTION; BATCH-COOLING CRYSTALLIZATION; CHORD-LENGTH DISTRIBUTIONS; L-GLUTAMIC ACID; ANTISOLVENT CRYSTALLIZATION; ANTI-SOLVENT; PREFERENTIAL CRYSTALLIZATION; INDUSTRIAL CRYSTALLIZATION; POLYMORPHIC TRANSFORMATION;

D O I：

10.1002/ceat.201100344

中图分类号：

TQ [化学工业];

学科分类号：

0817 ;

摘要：

Laser-backscattering instruments, such as the focused beam reflectance measurement or threefold dynamical optical reflectance measurement, are promising tools to aid crystallization process development, allowing an in situ, real-time, and nondestructive measurement of particle size distributions. Besides the instrument principles, in detail geometrical and optical models are discussed which deconvolute the recorded chord length distribution. Emphasis is thereby laid on the influence of the suspension density on instrument recordings. The application of laser-backscattering devices for determination of kinetic constants is discussed and future directions and perspectives are given.

引用

页码：967 / 979

页数：13

共 119 条

[21] Sizing polydisperse dispersions by focused beam reflectance and small angle static light scattering [J].

Ehrl, Lyonel ;

Soos, Miroslav ;

Morbidelli, Massimo .

PARTICLE & PARTICLE SYSTEMS CHARACTERIZATION, 2007, 23 (06) :438-447

[22]

Euhus D.D., 2003, Nucleation in bulk solutions and crystal growth on heat transfer surfaces during evaporative crystallization of salts composed of Na2CO4 and Na2SO4

[23] Paracetamol crystallization using laser backscattering and ATR-FTIR spectroscopy: Metastability, agglomeration, and control [J].

Fujiwara, M ;

Chow, PS ;

Ma, DL ;

Braatz, RD .

CRYSTAL GROWTH & DESIGN, 2002, 2 (05) :363-370

[24] INDUSTRIAL CRYSTALLIZATION FROM SOLUTION [J].

GARSIDE, J .

CHEMICAL ENGINEERING SCIENCE, 1985, 40 (01) :3-26

[25] Geometric figures with the same chord length probability density function: Six examples [J].

Gille, Wilfried .

POWDER TECHNOLOGY, 2009, 192 (01) :85-91

[26] In-line monitoring of crystallization processes using a laser reflection sensor and a neural network model [J].

Giulietti, M ;

Guardani, R ;

Nascimento, CAO ;

Arntz, B .

CHEMICAL ENGINEERING & TECHNOLOGY, 2003, 26 (03) :267-272

[27] Hydrate formation from high water content-crude oil emulsions [J].

Greaves, David ;

Boxall, John ;

Mulligan, James ;

Sloan, E. Dendy ;

Koh, Carolyn A. .

CHEMICAL ENGINEERING SCIENCE, 2008, 63 (18) :4570-4579

[28] Measuring the particle size of a known distribution using the focused beam reflectance measurement technique [J].

Greaves, David ;

Boxall, John ;

Mulligan, James ;

Montesi, Alberto ;

Creek, Jefferson ;

Sloan, E. Dendy ;

Koh, Carolyn A. .

CHEMICAL ENGINEERING SCIENCE, 2008, 63 (22) :5410-5419

[29] Polymer flocculation of calcite: Population balance model [J].

Heath, AR ;

Bahri, PA ;

Fawell, PD ;

Farrow, JB .

AICHE JOURNAL, 2006, 52 (05) :1641-1653

[30]

Heath AR, 2002, PART PART SYST CHAR, V19, P84, DOI 10.1002/1521-4117(200205)19:2<84::AID-PPSC84>3.0.CO

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