Synthesis and characterization of α-{3-[2-hydroxy-3-(N-methyl-N-hydroxy-ethylamino)propoxy]propyl}-ω-butylpolydimethylsiloxanes

被引：2

作者：

Sun, Hai Feng ^{[1
]}

Zhang, Qing Si ^{[1
]}

Zhang, Meng ^{[2
]}

Yu, Yi Tao ^{[1
]}

Zong, Jian Ping ^{[1
]}

机构：

[1] Shandong Inst Light Ind, Sch Chem Engn, Jinan 250100, Peoples R China

[2] Jiangnan Univ, Sch Chem & Mat, Wuxi 214122, Peoples R China

来源：

CHINESE CHEMICAL LETTERS | 2008年 / 19卷 / 10期

关键词：

Anionic ring-opening polymerization; Hydrosilylation; Epoxy addition; alpha-{3-[2-Hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl}-omega-butylpolydimethylsiloxanes;

D O I：

10.1016/j.cclet.2008.06.047

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

alpha-{3-[2-hydroxy-3-(N-methyl-N-hydroxyethylamino)propoxy]propyl}-omega-butylpolydimethylsiloxanes III with various molecular weights were prepared by epoxy addition of alpha-[3-(2,3-epoxy-propoxy)propyl]-omega-butylpolydimethylsiloxanes II and N-methylmonoethanolamine. At each step, the outcome compounds were characterized through FT-IR and NMR spectra, the results showed that each step was successfully carried out and objective products were achieved. (C) 2008 Qing Si Zhang. Published by Elsevier B. V. on behalf of Chinese Chemical Society. All rights reserved.

引用

页码：1196 / 1198

页数：3

共 25 条

[21] A simple synthesis of functionalized 3-methyl-1-pyridinyl-1H-imidazolium salts as bidentate N-heterocyclic-carbene precursors and their application in Ir-catalyzed arene borylation [J].

Peters, Martin ;

Breinbauer, Rolf .

TETRAHEDRON LETTERS, 2010, 51 (50) :6622-6625

[22] Fluorosubstituted rhodacarboranes 3,4-(R3P)2-3-H-3,1,2-RhC2B9H11−nFn (n=1, 2, 4): Synthesis, molecular structure, and catalytic properties in hydrosilylation of styrene and phenylacetylene [J].

V. N. Lebedev ;

E. V. Balagurova ;

F. M. Dolgushin ;

A. I. Yanovskii ;

L. I. Zakharkin .

Russian Chemical Bulletin, 1997, 46 :550-558

[23] Synthesis, light-harvesting and energy-transfer properties of regioregular silylene-spaced alternating [(donor-SiMe2-)n=1-3-(acceptor-SiMe2)] copolymers [J].

Cheng, YJ ;

Luh, TY .

CHEMISTRY-A EUROPEAN JOURNAL, 2004, 10 (21) :5361-5368

[24] Diverse catalytic activity of the cationic actinide complex [(Et2N)3U][BPh4] in the dimerization and hydrosilylation of terminal alkynes.: Characterization of the first f-element alkyne π-complex [(Et2N)2U(CCtBu)(η2-HCCtBu)][BPh4] [J].

Dash, AK ;

Wang, JX ;

Berthet, JC ;

Ephritikhine, M ;

Eisen, MS .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2000, 604 (01) :83-98

[25] Iminophosphines:: synthesis, formation of 2,3-dihydro-1H-benzo[1,3]azaphosphol-3-ium salts and N-(pyridin-2-yl)-2-diphenylphosphinoylaniline, coordination chemistry and applications in platinum group catalyzed Suzuki coupling reactions and hydrosilylations [J].

Doherty, S ;

Knight, JG ;

Scanlan, TH ;

Elsegood, MRJ ;

Clegg, W .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2002, 650 (1-2) :231-248

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