Synthesis and Crystal Structure of 1,2,4-Triazol-5(4H)-one Derivative

被引：0
|
作者：
Ye, Dong-Ju [1 ]
Feng, Xiao-Liang [1 ]
Zhang, Zheng-Hong [1 ]
机构：
[1] Quzhou Coll, Coll Chem & Mat Engn, Quzhou 324000, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2012年 / 24卷 / 11期
关键词：
Crystal structure; Synthesis; 1,2,4-Triazole; BIOLOGICAL-ACTIVITIES; CYCLOPROPANE MOIETY; DFT CALCULATION; DESIGN;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new triazole compound, C17H15N3OCl2, has been synthesized and the crystal structure was determined by a single crystal X-ray diffraction study. The crystal symmetry is monoclinic, space group P2(1)/n, with a = 8.1479(17) angstrom, b = 7.9177(17) angstrom, c = 25.774(5) angstrom, alpha = 90 degrees, beta = 92.976(4)degrees, gamma = 90 degrees. An extensive three-dimensional network was observed due to the pi-pi interactions.
引用
收藏
页码：5286 / 5288
页数：3
相关论文
共 50 条
  • [31] Synthesis and crystal structure of 1,4-bis(1H-1,2,4-triazol-1-methyl)benzene
    Peng, YF
    Li, BZ
    Zhou, JH
    Li, BL
    Zhang, Y
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2004, 23 (09) : 985 - 988
  • [32] Synthesis, Crystal Structure and Biological Activity of a New 1,2,4-Triazole Derivative
    Tong Jian-Ying
    Wu Hong-Ke
    Sun Na-Bo
    Liu Xing-Hai
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2013, 32 (04) : 607 - 611
  • [33] Synthesis and crystal structure of 4-phenyl-5-(1′t-butyl-5′-methyl-4′-pyrazolyl)-1,2,4-triazol-3-thione
    Ming, L
    Wen, LR
    Fu, WJ
    Wang, SW
    Yang, HZ
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2004, 23 (05) : 506 - 509
  • [34] Synthesis and Crystal Structure of 4-Salicyli deneamino-3-methyl-1,2,4-triazol-5-thione
    WEN Li-Ronga
    结构化学, 2003, (05) : 529 - 532
  • [35] Synthesis and Crystal Structure of 4-Phenyl-5-(1't-butyl-5'-methyl-4'-pyrazolyl)-1,2,4-triazol-3-thione
    LI Minga
    结构化学, 2004, (05) : 506 - 509
  • [36] Synthesis,Crystal Structure and Biological Activity of 2-Chloro-5-(((5-(1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl)-4-phenyl-4H-1,2,4-triazol-3-yl)thio)methyl)thiazole
    沈钟华
    翟志文
    孙召慧
    翁建全
    谭成侠
    刘幸海
    结构化学, 2017, 36 (07) : 1137 - 1141
  • [37] Synthesis and Biological Study of 3-Butyl-1-(2,6-dichlorophenyl)-1H-[1,2,4]triazol-5(4H)-one Derivatives as Anti-hypertension Drugs
    Zhang, Yanchun
    Zhou, Jinpei
    Pan, Weihong
    Wu, Xiaoming
    Wang, Shuai
    LETTERS IN DRUG DESIGN & DISCOVERY, 2010, 7 (01) : 18 - 22
  • [38] Synthesis and characterization of novel triazol compounds containing a thiophen ring as potential antifungal agents and the structure of 2-(2-hydroxy-2-p-tolyethyl)-5-(thiophen-2-ylmethyl)-4-(4H-1,2,4-triazol-4-yl)-2H-1,2,4-triazol-3(4H)-one
    Unver, Yasemin
    Dugdu, Esra
    Sancak, Kemal
    Er, Mustafa
    Ustabas, Resat
    TURKISH JOURNAL OF CHEMISTRY, 2010, 34 (04) : 551 - 563
  • [39] Synthesis, Crystal Structure and Antitumor Activity of 2-(3-Methyl-5-(methylthio)-4H-1,2,4-triazol-4-yl)isoindoline-1,3-dione
    Zhao Pei-Liang
    Hu Meng-Jin
    Duan An-Na
    Sun Xiao-Min
    You Wen-Wei
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2015, 34 (03) : 359 - 364
  • [40] An Unexpected Product N-(3-((2-fluorobenzyl)thio)-5-methyl-4H-1,2,4-triazol-4-yl)acetimidamide: Synthesis and Structure Analysis
    Sun, Na-Bo
    Liu, Xing-Hai
    Weng, Jian-Quan
    Tan, Cheng-Xia
    JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN, 2013, 35 (02): : 499 - 502
12345