Optimization of matrix solid-phase dispersion extraction for the chromatographic analysis of flavones in cranberries

被引:0
作者
Linkeviciute, Ausra [1 ,2 ]
Butkiene, Rita [2 ]
Naujalis, Evaldas [1 ,2 ]
机构
[1] Vilnius State Univ, Dept Analyt & Environm Chem, LT-03225 Vilnius, Lithuania
[2] Ctr Phys Sci & Technol, State Res Inst, LT-01108 Vilnius, Lithuania
来源
CHEMIJA | 2013年 / 24卷 / 03期
关键词
matrix solid-phase dispersion (MSPD); cranberry; myricetin; quercetin; kaempferol; HPLC-MS; VACCINIUM-MACROCARPON; PHENOLIC-COMPOUNDS; IN-VITRO; PROANTHOCYANIDINS; ANTIOXIDANT; PRODUCTS; FRUITS; MS;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A matrix solid-phase dispersion (MSPD) extraction method was applied for three flavones in cranberry (Vaccinium macrocarpon Ait.) matrix for the first time. The optimized MSPD procedure required a small amount of the sample (0.25 g), C18 bonded silica gel (1.0 g) as a dispersant solid-phase sorbent and small volumes of methanol using its aqueous solutions (10 mL) as eluting solvents. Identification and quantification of myricetin, quercetin and kaempferol were performed by HPLC-DAD-MS. The limit of detection varies from 0.04 mu g/g to 0.08 mu g/g with linear regression coefficients (r(2) > 0.999) for each compound. The recoveries of the analytes ranging from 59% to 111% with relative standard deviations less than 9.5% were checked using spiked freezedried cranberry samples. The MSPD method is simple, rapid and efficient for the extraction of flavones from cranberry samples.
引用
收藏
页码:217 / 222
页数:6
相关论文
共 50 条
  • [21] Application of matrix solid-phase dispersion to the determination of a new generation of fungicides in fruits and vegetables
    Navarro, M
    Picó, Y
    Marín, R
    Mañes, J
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2002, 968 (1-2) : 201 - 209
  • [22] A simple; efficient and environmentally friendly method for the extraction of pesticides from onion by matrix solid-phase dispersion with liquid chromatography-tandem mass spectrometric detection
    Rodrigues, Sherol Acosta
    Caldas, Sergiane Souza
    Primel, Ednei Gilberto
    [J]. ANALYTICA CHIMICA ACTA, 2010, 678 (01) : 82 - 89
  • [23] A rapid method for the analysis of perfluorinated alkyl substances in serum by hybrid solid-phase extraction
    Honda, Masato
    Robinson, Morgan
    Kannan, Kurunthachalam
    [J]. ENVIRONMENTAL CHEMISTRY, 2018, 15 (1-2) : 92 - 99
  • [24] A reversed-phase high-performance liquid chromatography method combined with matrix solid-phase dispersion extraction for the determination of teflubenzuron, lufenuron and bifenthrin residues in lyophilized coconut water
    Santana Santos, Luis Fabricio
    da Silva Souza, Nicaellen Roberta
    Ferreira, Jordana Alves
    Navickiene, Sandro
    [J]. JOURNAL OF FOOD COMPOSITION AND ANALYSIS, 2012, 26 (1-2) : 183 - 188
  • [25] Application of Matrix Solid-Phase Dispersion and Liquid Chromatography–Ion Trap Mass Spectrometry for the Analysis of Pesticide Residues in Fruits
    Marina M. Radišić
    Tatjana M. Vasiljević
    Nikolina N. Dujaković
    Mila D. Laušević
    [J]. Food Analytical Methods, 2013, 6 : 648 - 657
  • [26] Analysis of multi-class preservatives in leave-on and rinse-off cosmetics by matrix solid-phase dispersion
    Sanchez-Prado, Lucia
    Alvarez-Rivera, Gerardo
    Pablo Lamas, J.
    Lores, Marta
    Garcia-Jares, Carmen
    Llompart, Maria
    [J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2011, 401 (10) : 3293 - 3304
  • [27] Simultaneous extraction, separation, isolation and identification of endogenous components from Etlingera elatior by pressurized matrix solid-phase dispersion using liquid chromatography-mass spectrometry
    Ge, Liya
    Yong, Jean Wan Hong
    Tan, Swee Ngin
    Li, Shao-Ping
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2020, 1611
  • [28] Development and Validation of a Matrix Solid-Phase Dispersion Method to Determine Acrylamide in Coffee and Coffee Substitutes
    Dias Soares, Cristina M.
    Alves, Rita C.
    Casal, Susana
    Oliveira, M. Beatriz P. P.
    Fernandes, Jose Oliveira
    [J]. JOURNAL OF FOOD SCIENCE, 2010, 75 (03) : T57 - T63
  • [29] Simultaneous determination of phenolic compounds in Equisetum palustre L. by ultra high performance liquid chromatography with tandem mass spectrometry combined with matrix solid-phase dispersion extraction
    Wei, Zuofu
    Pan, Youzhi
    Li, Lu
    Huang, Yuyang
    Qi, Xiaolin
    Luo, Meng
    Zu, Yuangang
    Fu, Yujie
    [J]. JOURNAL OF SEPARATION SCIENCE, 2014, 37 (21) : 3045 - 3051
  • [30] Simultaneous microextraction of inorganic iodine and iodinated amino acids by miniaturized matrix solid-phase dispersion with molecular sieves and ionic liquids
    Cao, Jun
    Peng, Li-Qing
    Xu, Jing-Jing
    Du, Li-Jing
    Zhang, Qi-Dong
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2016, 1477 : 1 - 10