Preparation of Graphene-ZrO2 Nanocomposites by Heat Treatment and Photocatalytic Degradation of Organic Dyes

被引:26
作者
Cho, Bum Hwi [1 ]
Ko, Weon Bae [1 ]
机构
[1] Sahmyook Univ, Dept Chem, Seoul 139742, South Korea
关键词
ZrO2; Nanoparticles; Graphene; Organic Dyes; Graphene-ZrO2; Nanocomposites; Photocatalytic Degradation; ELECTRIC FURNACE; TIO2; NANOPARTICLES;
D O I
10.1166/jnn.2013.7819
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
ZrO2 nanoparticles were synthesized by combining a solution containing zinconyl chloride in distilled water with a NH4OH solution under microwave irradiation. Graphene and ZrO2 nanocomposites were synthesized in an electric furnace at 700 degrees C for 2 hours. The heated graphene-ZrO2 nanocomposites were characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. In addition, UV-vis spectrophotometry was used to evaluate the heated graphene-ZrO2 nanocomposites as a catalyst in the photocatalytic degradation of organic dyes. The photocatalytic effect of the heated graphene-ZrO2 nanocomposites was compared with that of unheated graphene nanoparticles, heated graphene nanoparticles, and unheated graphene-ZrO2 nanocomposites in organic dyes (methylene blue, methyl orange, and rhodamine B) under ultraviolet light at 254 nm.
引用
收藏
页码:7625 / 7630
页数:6
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