Rapid Synthesis of DDR Zeolite at Room Temperature

被引：23

作者：

Sen, Mitali ^{[1
]}

Bose, Ankita ^{[1
]}

Pal, Pameli ^{[1
]}

Das, Jugal K. ^{[1
]}

Das, Nandini ^{[1
]}

机构：

[1] Cent Glass & Ceram Res Inst, CSIR, Ceram Membrane Div, Kolkata 700032, India

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2014年 / 97卷 / 01期

关键词：

SONOCHEMICAL SYNTHESIS; SEPARATION; DD3R;

D O I：

10.1111/jace.12687

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

In this work, DDR zeolites were synthesized by sonochemical method without the application of any heat energy at room temperature. The synthesized zeolites were characterized by X-ray diffraction (XRD), infrared (IR) spectral analysis, and field-emission scanning electron microscopy (FESEM). XRD and IR results showed that phase pure DDR zeolite was started to form at room temperature after 24 h of aging and completed the formation after 5 d of aging. The Brunauer-Emmett-Teller (BET) surface area of the powder was found to be 202 m(2)/g. The FESEM micrograph and elemental analysis showed that desired atomic ratio of the DDR zeolite was obtained after 5 days of synthesis.

引用

页码：52 / 55

页数：4

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