Development of a semi-automated system for routine preparation of carbonate samples

被引：0
|
作者：
Tisnérat-Laborde, N [1 ]
Poupeau, JJ [1 ]
Tannau, JF [1 ]
Paterne, M [1 ]
机构：
[1] CEA, CNRS, Lab Sci Climat & Environm, UMR 1572, F-91198 Gif Sur Yvette, France
来源：
RADIOCARBON | 2001年 / 43卷 / 2A期
关键词：
D O I：
暂无
中图分类号：
P3 [地球物理学]; P59 [地球化学];
学科分类号：
0708 ; 070902 ;
摘要：
We constructed a semi-automated system to transform carbonate samples to CO2, as a means to increase sample-processing capacity. The physico-chemical process includes hydrolysis of carbonate, quantification of the mass of carbon and CO2 collection in a glass ampoule. The system is computer-controlled and monitored, and all the data are stored. A single run of five consecutive samples requires about 3.5 hours. Measurements of C-14 concentrations were made on samples of IAEA C-1 Carrara marble to test the reliability of this semi-automated system. These measurements have allowed the determination of the total system background and the memory effect of our system.
引用
收藏
页码：299 / 304
页数：6
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