Synthesis of zeolite membrane (MCM-22/α-alumina) and its application in the process of oil-water separation

被引:10
作者
Barbosa, Antonielly S. [1 ]
Barbosa, Antusia S. [1 ]
Rodrigues, Meiry G. F. [1 ]
机构
[1] Univ Fed Campina Grande, Acad Unit Chem Engn, BR-58109970 Campina Grande, Brazil
关键词
MCM-22 zeolite membrane; Rubbing; -Al2O3; Oil-water; WASTE-WATER; MICROFILTRATION; PERFORMANCE;
D O I
10.1080/19443994.2014.995719
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Zeolite membrane (MCM-22/-Al2O3) was prepared on -Al2O3 disk by synthesis method (rubbing) and investigated through water separation and oily water recovery. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and mercury porosimetry. Thereafter, the separation of oil-water emulsion was evaluated. The crystallization behavior of the particles of the zeolite membrane is observed through the XRD. The images obtained by SEM of the zeolite membrane (MCM-22/-Al2O3) showed that the method used for the synthesis of the zeolite membrane was effective since it showed the formation of a homogeneous surface with no cracks or defects on the surface of the porous support of -Al2O3. Oil rejection was monitored. Fouling occurred as a layer on the membrane surface. The test showed that the MCM-22 zeolite membrane has potential for oil-water separation.
引用
收藏
页码:3665 / 3672
页数:8
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