Exploring nanomaterials with 3D electron microscopy

被引:61
作者
Ersen, O. [1 ]
Florea, I. [1 ,3 ]
Hirlimann, C. [1 ]
Pham-Huu, C. [2 ]
机构
[1] Univ Strasbourg, IPCMS, CNRS, UMR 7504, F-67034 Strasbourg 2, France
[2] Univ Strasbourg, ECPM, CNRS, ICPEES,UMR 7515, F-67087 Strasbourg 2, France
[3] Ecole Polytech, CNRS, LPICM, UMR 7647, F-91128 Palaiseau, France
关键词
3-DIMENSIONAL RECONSTRUCTION; MESOPOROUS SILICA; NANOCRYSTAL SUPERLATTICES; CARBON NANOTUBES; RADIATION-DAMAGE; IMAGE-ANALYSIS; ATOM-PROBE; TOMOGRAPHY; NANOPARTICLES; RESOLUTION;
D O I
10.1016/j.mattod.2015.04.004
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this review we focus on recent developments in the field of 3D imaging at the nanoscale, when applied to nanomaterials and nanostructures. We demonstrate, by highlighting examples, that recent progress in the use of electron microscopy techniques based on tomography allows one to fill the gap between the development of new materials and their structures and characterization. A special emphasis is put on two new 3D approaches: quantitative and analytical 3D tomography. The first approach gives access to the quantitative exploration of specific parameters within nano-objects and/or nanostructures while the latter, based on electron energy loss spectroscopy, details the 3D chemical composition of such systems at the nanometre scale.
引用
收藏
页码:395 / 408
页数:14
相关论文
共 91 条
[1]   Cryo-transmission electron microscopy of Ag nanoparticles grown on an ionic liquid substrate [J].
Anjum, Dalaver H. ;
Stiger, Rebecca M. ;
Finley, James J. ;
Conway, James F. .
JOURNAL OF MATERIALS RESEARCH, 2010, 25 (07) :1264-1271
[2]   High-Density Monodispersed Cobalt Nanoparticles Filled into Multiwalled Carbon Nanotubes [J].
Baaziz, Walid ;
Begin-Colin, Sylvie ;
Pichon, Benoit P. ;
Florea, Ileana ;
Ersen, Ovidiu ;
Zafeiratos, Spyridon ;
Barbosa, Roland ;
Begin, Dominique ;
Pham-Huu, Cuong .
CHEMISTRY OF MATERIALS, 2012, 24 (09) :1549-1551
[3]   Quantitative three-dimensional reconstruction of catalyst particles for bamboo-like carbon nanotubes [J].
Bals, Sara ;
Batenburg, K. Joost ;
Verbeeck, Jo ;
Sijbers, Jan ;
Van Tendeloo, Gustaaf .
NANO LETTERS, 2007, 7 (12) :3669-3674
[4]   3D imaging of nanomaterials by discrete tomography [J].
Batenburg, K. J. ;
Bals, S. ;
Sijbers, J. ;
Kuebel, C. ;
Midgley, P. A. ;
Hernandez, J. C. ;
Kaiser, U. ;
Encina, E. R. ;
Coronado, E. A. ;
Van Tendeloo, G. .
ULTRAMICROSCOPY, 2009, 109 (06) :730-740
[5]   Magnetic Properties of Annealed Core-Shell CoPt Nanoparticles [J].
Bigot, Jean-Yves ;
Kesserwan, Hasan ;
Halte, Valerie ;
Ersen, Ovidiu ;
Moldovan, M. Simona ;
Kim, Tae Hee ;
Jang, Jung-tak ;
Cheon, Jinwoo .
NANO LETTERS, 2012, 12 (03) :1189-1197
[6]   AN ATOM-PROBE FOR 3-DIMENSIONAL TOMOGRAPHY [J].
BLAVETTE, D ;
BOSTEL, A ;
SARRAU, JM ;
DECONIHOUT, B ;
MENAND, A .
NATURE, 1993, 363 (6428) :432-435
[7]   The Rose model, revisited [J].
Burgess, AE .
JOURNAL OF THE OPTICAL SOCIETY OF AMERICA A-OPTICS IMAGE SCIENCE AND VISION, 1999, 16 (03) :633-646
[8]   Atom probe tomography today [J].
Cerezo, Alfred ;
Clifton, Peter H. ;
Galtrey, Mark J. ;
Humphreys, Colin J. ;
Kelly, Thomas F. ;
Larson, David J. ;
Lozano-Perez, Sergio ;
Marquis, Emmanuelle A. ;
Oliver, Rachel A. ;
Sha, Gang ;
Thompson, Keith ;
Zandbergen, Mathijs ;
Alvis, Roger L. .
MATERIALS TODAY, 2007, 10 (12) :36-42
[9]   Three-dimensional imaging of dislocations in a nanoparticle at atomic resolution [J].
Chen, Chien-Chun ;
Zhu, Chun ;
White, Edward R. ;
Chiu, Chin-Yi ;
Scott, M. C. ;
Regan, B. C. ;
Marks, Laurence D. ;
Huang, Yu ;
Miao, Jianwei .
NATURE, 2013, 496 (7443) :74-+
[10]   On Resolution in Electron Tomography of Beam Sensitive Materials [J].
Chen, Delei ;
Friedrich, Heiner ;
de With, Gijsbertus .
JOURNAL OF PHYSICAL CHEMISTRY C, 2014, 118 (02) :1248-1257