Preparation of Silver Nanoparticles and Antibiotic Test of Its Polycarbonate Films Composite

被引:7
|
作者
Lee, Sang Hyun [1 ,2 ]
Sung, Kiwhan [1 ]
Chung, Taek-Mo [1 ]
Lee, Sung-Goo [1 ]
Min, Kyung Dae [1 ]
Koo, Sangman [2 ]
Kim, Chang Gyoun [1 ]
机构
[1] Korea Res Inst Chem Technol, Adv Mat Div, Taejon 305600, South Korea
[2] Hanyang Univ, Dept Chem Engn, Seoul 133791, South Korea
关键词
Nanocatalysis; Silver Nanoparticles; Organic Nano Sol; Antifungal Effect;
D O I
10.1166/jnn.2008.IC55
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
General synthetic methods for silver nanoparticles are reduction of metal salt in aqueous solution or alcoholic solution. However, the preparation of silver nanoparticles in organic solvent is rarely reported. The most common preparation methods for silver nanoparticles in organic solvent are based on transfer of nanoparticles from aqueous phase to organic phase by phase transfer agent. We describe an easy synthetic method to prepare dispersed silver nanoparticles (similar to 10 nm) by reduction of silver cation in organic solvent such as toluene using a reducing agent and a capping agent. The synthesized silver nanoparticles and polycarbonate were mixed and molded to prepare a new composite in methylene chloride. The composite was tested to investigate antifungal effect by coliform (Escherichia coli ATCC 25922). The antifungal effect of the composite reached high after 24 h (99.9999%). The composite and the silver nanoparticles have been characterized using X-ray diffraction (XRD), UV-vis spectroscopy, transmission electron microscopy (TEM), and inductively coupled plasma (ICP).
引用
收藏
页码:4734 / 4737
页数:4
相关论文
共 50 条
  • [1] Tocopherol-mediated synthesis of silver nanoparticles and preparation of antimicrobial PBAT/silver nanoparticles composite films
    Shankar, Shiv
    Rhim, Jong-Whan
    LWT-FOOD SCIENCE AND TECHNOLOGY, 2016, 72 : 149 - 156
  • [2] Amino acid mediated synthesis of silver nanoparticles and preparation of antimicrobial agar/silver nanoparticles composite films
    Shankar, Shiv
    Rhim, Jong-Whan
    CARBOHYDRATE POLYMERS, 2015, 130 : 353 - 363
  • [3] Preparation of composite films with silver nanoparticles and their fractal aggregates in a polymeric matrix
    I. R. Saifullina
    G. A. Chiganova
    S. V. Karpov
    V. V. Slabko
    Russian Journal of Applied Chemistry, 2006, 79 : 1639 - 1642
  • [4] Preparation and characterization of agar/silver nanoparticles composite films with antimicrobial activity
    Rhim, J. W.
    Wang, L. F.
    Hong, S. I.
    FOOD HYDROCOLLOIDS, 2013, 33 (02) : 327 - 335
  • [5] Preparation of composite films with silver nanoparticles and their fractal aggregates in a polymeric matrix
    Saifullina, I. R.
    Chiganova, G. A.
    Karpov, S. V.
    Slabko, V. V.
    RUSSIAN JOURNAL OF APPLIED CHEMISTRY, 2006, 79 (10) : 1639 - 1642
  • [6] Preparation of Biodegradable Polymer/Silver Nanoparticles Composite and Its Antibacterial Efficacy
    Kim, Jonghoon
    Lee, Jungeun
    Kwon, Soonchul
    Jeong, Sunghoon
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2009, 9 (02) : 1098 - 1102
  • [7] Kinetics of the thermal degradation of polycarbonate films containing silver nanoparticles
    N. N. Volkova
    L. M. Bogdanova
    L. I. Kuzub
    N. N. Dremova
    Polymer Science Series B, 2015, 57 : 31 - 38
  • [8] One-step preparation of banana powder/silver nanoparticles composite films
    Aungkana Orsuwan
    Shiv Shankar
    Long-Feng Wang
    Rungsinee Sothornvit
    Jong-Whan Rhim
    Journal of Food Science and Technology, 2017, 54 : 497 - 506
  • [9] Preparation and characterization of cinnamaldehyde/polyvinyl alcohol/silver nanoparticles ternary composite films
    Gao, Hongfang
    Yang, Hui
    INTERNATIONAL JOURNAL OF POLYMER ANALYSIS AND CHARACTERIZATION, 2021, 26 (01) : 24 - 36
  • [10] One-step preparation of banana powder/silver nanoparticles composite films
    Orsuwan, Aungkana
    Shankar, Shiv
    Wang, Long-Feng
    Sothornvit, Rungsinee
    Rhim, Jong-Whan
    JOURNAL OF FOOD SCIENCE AND TECHNOLOGY-MYSORE, 2017, 54 (02): : 497 - 506