Synthesis, crystal structure and thermoanalysis of bis{[μ-bis-N,N′-(2-hydroxybenzoyl)-1,3-propandiaminato](N,N′-dimethyl formamide) (μ- benzoato)nickel(II)}nickel(II)

被引：11

作者：

Akay, Abdulkadir

Arici, Cengiz ^{[1
]}

Atakol, Orhan

Fuess, Hartmut

Svoboda, Ingrid

机构：

[1] Hacettepe Univ, Dept Engn Phys, TR-06532 Ankara, Turkey

[2] Ankara Univ, Dept Chem, TR-06100 Ankara, Turkey

[3] Tech Univ Darmstadt, FB Materialwissensch, D-64287 Darmstadt, Germany

来源：

JOURNAL OF COORDINATION CHEMISTRY | 2006年 / 59卷 / 08期

关键词：

homotrinuclear complex; nickel(II); reduced Schiff base; thermogravimetric analysis; crystal structure;

D O I：

10.1080/00958970500410374

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The title compound is a centrosymmetric, linear, homotrinuclear nickel(II) complex and has been characterized by elemental and thermogravimetric analysis, IR spectroscopy and single-crystal X-ray diffraction. The complex is monoclinic, space group P2(1)/n, with a = 13.707(4), b = 13.455(2), c = 14.620(3) angstrom, beta = 101.300(2)degrees, V = 2644.1(10) angstrom(3) and Z = 2. The central and terminal nickel( II) ions have distorted octahedral geometry with a Ni center dot center dot center dot Ni distance of 3.047(1) angstrom.

引用

页码：933 / 938

页数：6

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