A Convenient Deoxygenation-Dimerization-[1+2]-Cycloaddition Synthetic Sequence from ω-Bromoalkylisatins to Indolin-2-onemethanofullerenes Bearing Isoindigo Moiety

被引：10

作者：

Bogdanov, Andrei V. ^{[1
]}

Yusupova, Gulshat G. ^{[1
]}

Romanova, Irina P. ^{[1
]}

Latypov, Shamil K. ^{[1
]}

Krivolapov, Dmitry B. ^{[1
]}

Mironov, Vladimir F. ^{[1
]}

Sinyashin, Oleg G. ^{[1
]}

机构：

[1] Russian Acad Sci, AE Arbuzov Inst Organ & Phys Chem, Kazan Res Ctr, Kazan 420088, Russia

来源：

SYNTHESIS-STUTTGART | 2013年 / 45卷 / 05期

关键词：

phosphorus; deoxygenation; carbenes; cycloaddition; fullerenes; NMR-SPECTROSCOPY; DERIVATIVES; ISATINS; DESIGN; ACENAPHTHENEQUINONE; CHEMISTRY; ROUTE;

D O I：

10.1055/s-0032-1316844

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

An easy and convenient step-by-step synthetic procedure towards the design of a novel spiroindolomethanofullerene bearing an isoindigo fragment is reported.

引用

页码：668 / 672

页数：5

共 47 条

[1]

[Anonymous], 1989, ONE 2 DIMENSIONAL NM

[2] Structure-NMR chemical shift relationships for novel functionalized derivatives of quinoxalines [J].

Balandina, A ;

Kalinin, A ;

Mamedov, V ;

Figadère, B ;

Latypov, S .

MAGNETIC RESONANCE IN CHEMISTRY, 2005, 43 (10) :816-828

[3] THE STRUCTURE AND PROPERTIES OF SOME INDOLIC CONSTITUENTS IN COUROUPITA-GUIANENSIS AUBL [J].

BERGMAN, J ;

LINDSTROM, JO ;

TILSTAM, U .

TETRAHEDRON, 1985, 41 (14) :2879-2881

[4] Determination of relative configuration in organic compounds by NMR spectroscopy and computational methods [J].

Bifulco, Giuseppe ;

Dambruoso, Paolo ;

Gomez-Paloma, Luigi ;

Riccio, Raffaele .

CHEMICAL REVIEWS, 2007, 107 (09) :3744-3779

[5] FACILE AND CONVENIENT SYNTHESIS OF FUNCTIONALIZED ARYL-CONTAINING ISOINDIGO DERIVATIVES VIA SUBSTITUTED INDOLIN-2-ONE CARBENE DIMERIZATION [J].

Bogdanov, Andrei V. ;

Mironov, Vladimir F. ;

Musin, Lenar I. ;

Musin, Rashid Z. ;

Krivolapov, Dmitry B. ;

Litvinov, Igor A. .

SYNTHETIC COMMUNICATIONS, 2012, 42 (16) :2388-2395

[6] A convenient synthetic route from isatin N-Mannich bases to nitrogen-containing derivatives of isoindigo [J].

Bogdanov, Andrei V. ;

Mironov, Vladimir F. ;

Musin, Lenar I. ;

Musin, Rashid Z. ;

Krivolapov, Dmitry B. ;

Litvinov, Igor A. .

MONATSHEFTE FUR CHEMIE, 2011, 142 (01) :81-85

[7] Facile Synthesis of 1,1′-Dialkylisoindigos through Deoxygenation Reaction of Isatins and Tris(diethylamino)phosphine [J].

Bogdanov, Andrei V. ;

Mironov, Vladimir F. ;

Musin, Lenar I. ;

Musin, Rashid Z. .

SYNTHESIS-STUTTGART, 2010, (19) :3268-3270

[8] Deoxygenation of acenaphthenequinone with hexaethylphosphorous triamide: An efficient method of synthesis of biacenaphthylidenedione [J].

Bogdanov, AV ;

Mironov, VF ;

Buzykin, BI ;

Konovalov, AI .

RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2005, 75 (05) :825-826

[9] Biological evaluation of glycosyl-isoindigo derivatives against the pathogenic agents of tropical diseases (malaria, Chagas disease, leishmaniasis and human African trypanosomiasis) [J].

Bouchikhi, Fadoua ;

Anizon, Fabrice ;

Brun, Reto ;

Moreau, Pascale .

BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2011, 21 (21) :6319-6321

[10] Synthesis and evaluation of isatins and thiosemicarbazone derivatives against cruzain, falcipain-2 and rhodesain [J].

Chiyanzu, I ;

Hansell, E ;

Gut, J ;

Rosenthal, PJ ;

McKerrow, JH ;

Chibale, K .

BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2003, 13 (20) :3527-3530

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