Synthesis of ZnO, SnO2 Nanoparticles and Preparation of ZnO-SnO2 Nanocomposites

被引:4
作者
Gultekin, Deniz [1 ]
Alaf, Mirac [1 ]
Guler, Mehmet Oguz [1 ]
Akbulut, Hatenn [1 ]
机构
[1] Sakarya Univ, Met & Mat Engn Dept, Fac Engn, TR-54187 Sakarya, Turkey
关键词
ZnO; SnO2; Precipitation; Nanopowder; THIN-FILMS; OPTICAL-PROPERTIES; AL; PRECIPITATION; TEMPERATURE; PARTICLES; PERFORMANCE; DEPOSITION; POWDERS; PH;
D O I
10.1166/jnn.2012.6752
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
This article reports the preparation of ZnO-SnO2 nanocomposites from ZnO and SnO2 nanoparticles produced by homogenous precipitation route. Zinc acetate dihydrate (Zn(CH3COO)(2)center dot 2H(2)O) and tin(II) chloride dehydrates (SnCl2 center dot 2H(2)O) have been used as precursors. Distilled water was used as a solvent, monoethanolamine (MEA) is used as sol stabilizer. Precursors individually dissolved and stirred at 60 degrees C for 1 h. Certain amount of MEA were added to solution and stirred for 2 h. Then solution was cooled to room temperature and gets precipitated. The collected nanosized precipitates were mixed together and deposited on glass substrates by drain coating and post-heated at different temperatures. X-ray diffractometer was used to determine preferred crystal orientation and particle size of the thin films. Morphologies of nanopowders were examined by scanning electron microscope (SEM).
引用
收藏
页码:9175 / 9182
页数:8
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