Crystal structure of (E)-N-((2S,3S,4R,10R,13S,17S)-17-(1-(dimethylamino)ethyl)-2,4-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)-2-methylbut-2-enamide, C24H48N2O3

被引：0

作者：

Wu, Qi-Yun ^{[1
,2
,3
]}

Wu, Ji-Chun ^{[1
]}

Huo, Shao-Jie ^{[1
]}

He, Xi-Chen ^{[1
]}

Du, Jiang ^{[1
,2
,3
]}

机构：

[1] Guiyang Coll Tradit Chinese Med, Guiyang 550025, Guizhou, Peoples R China

[2] Key Lab Miao Med Guizhou Prov, Guiyang 550025, Guizhou, Peoples R China

[3] Guiyang Coll Tradit Chinese Med, Coll Pharm, Guiyang 550025, Guizhou, Peoples R China

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2019年 / 234卷 / 03期

基金：

中国国家自然科学基金;

关键词：

STEROIDAL ALKALOIDS;

D O I：

10.1515/ncrs-2018-0511

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

C24H48N2O3, monoclinic, P2(1) (no. 4), a = 14.805(3) angstrom, b = 10.0557(18) angstrom, c = 18.061(3) angstrom, beta = 98.935(5)degrees, V = 2656.3(8) angstrom(3), Z = 4, R-gt(F) = 0.0674, wR(ref)(F-2) = 0.1955, T = 173 K.

引用

页码：513 / 516

页数：4

共 6 条

[1] Adhikari A, 2015, NAT PROD COMMUN, V10, P1533
[2] Cholinesterase inhibiting and antiplasmodial steroidal alkaloids from Sarcococca hookeriana
Devkota, Krishna Prasad
Lenta, Bruno Ndjakou
Choudhary, Muhammad Iqbal
Naz, Qamar
Fekam, Fabrice Boyom
Rosenthal, Philip Joseph
Sewald, Norbert
[J]. CHEMICAL & PHARMACEUTICAL BULLETIN, 2007, 55 (09) : 1397 - 1401
[3] Bioactive Steroidal Alkaloids from Sarcococca hookeriana
Devkota, Krishna Prasad
Wansi, Jean D.
Lenta, Bruno N.
Khan, Samreen
Choudhary, Muhammad I.
Sewald, Norbert
[J]. PLANTA MEDICA, 2010, 76 (10) : 1022 - 1025
[4] OLEX2: a complete structure solution, refinement and analysis program
Dolomanov, Oleg V.
Bourhis, Luc J.
Gildea, Richard J.
Howard, Judith A. K.
Puschmann, Horst
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2009, 42 : 339 - 341
[5] Crystal structure of (Z)-N-(17-(1-(dimethylamino)ethyl)-10,13-dimethyl-4-oxo-4,5,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta-[a]phenanthren-3-yl)-3-methylbut-2-enimidic acid dichloromethane monosolvate, C29H45Cl2N2O2
He, Kang
Zou, Juan
Wang, Jin Xi
Du, Jiang
[J]. ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2013, 228 (03): : 327 - 328
[6] Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S2053273314026370, 10.1107/S0108767307043930]

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