Method Validation of 16 Types of Structural Amino Acids using an Automated Amino Acid Analyzer

被引：31

作者：

Shim, You-Shin ^{[1
]}

Yoon, Won-Jin ^{[1
,2
]}

Ha, Jaeho ^{[1
]}

Seo, Dongwon ^{[1
]}

Lee, Kwang-Won ^{[2
]}

Lee, Woo-Young ^{[3
]}

Kwon, Kwang-Il ^{[4
]}

Kang, Tae-Seok ^{[5
]}

Lee, Jin-Ha ^{[5
]}

Kim, Hyun-Jeong ^{[6
]}

Kwak, Hae-Jung ^{[6
]}

Lee, Sam-Pin ^{[6
]}

Kim, So-Jung ^{[7
]}

Yun, Won-Kap ^{[7
]}

Lee, Junsoo ^{[8
]}

Hwang, Jin-Bong ^{[1
]}

机构：

[1] Korea Food Res Inst, Food Anal Ctr, Gyeonggi 463746, South Korea

[2] Korea Univ, Coll Life Sci & Biotechnol, Seoul 136701, South Korea

[3] Nutr Safety Policy Div, Food Nutr & Dietary Safety Bur, Minist Food & Drug safety, Chungbuk 363700, South Korea

[4] Dietary Life Safety Div, Food Nutr & Dietary Safety Bur, Minist Food & Drug safety, Chungbuk 363700, South Korea

[5] Natl Inst Food & Drug safety Evaluat, Food safety Evaluat Dept, Chungbuk 363700, South Korea

[6] Keimyung Univ, Ctr Tradit Microorganism Resource, Taegu 704701, South Korea

[7] Gyeongbuk Inst Marine Bioind, Gyeongbuk 767813, South Korea

[8] Chungbuk Natl Univ, Dept Food Sci & Technol, Chungbuk 361763, South Korea

来源：

FOOD SCIENCE AND BIOTECHNOLOGY | 2013年 / 22卷 / 06期

关键词：

amino acids; automated amino acid analyzer; analytical method; validation; post column reaction; CHROMATOGRAPHY-MASS-SPECTROMETRY; PRECOLUMN DERIVATIZATION; PERFORMANCE; DERIVATIVES; MS/MS; FLUIDS; SERUM;

D O I：

10.1007/s10068-013-0252-0

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

An analytical method for the simultaneous determination of 16 types of structural amino acids in infant formula using an automated amino acid analyzer was validated through tests of precision, accuracy and linearity. The automated analysis of the amino acids was performed on an ion-exchange packed column with a visible detector. The certificated reference material (CRM) 1546 from NIST was used as the test sample to determine the precision and accuracy of the analytical method. The regression analyses revealed good correlations [correlation coefficient (r(2))] that were greater than 0.99. The recovery values of the amino acids were ranged from 87.18 to 118.08%. The limits of detection and limits of quantification were less than 0.059 mg/100 g and less than 0.198 mg/100 g, respectively. The infra- and inter-day precisions were less than 14.62% in the CRM sample.

引用

页码：1567 / 1571

页数：5

共 50 条

[41] DETERMINATION OF SEVERAL AMMONIA OR AMINO ACID SAMPLES ON ONE CHROMATOGRAM WITH AN AMINO ACID ANALYZER
SEELY, JH
EDATTEL, R
BENOITON, NL
JOURNAL OF CHROMATOGRAPHY, 1969, 45 (01): : 52 - &
[42] Plasma amino acid analysis by tandem mass spectrometry: A comparison to amino acid analyzer
Sokoro, AbdulRazaq
Lehotay, Denis C.
Hunter, Wayne
Schneider, Diana
FASEB JOURNAL, 2007, 21 (05): : A266 - A266
[43] Comparative Analysis of Some Essential Amino Acids and Available Lysine in Acacia colei and A. tumida Seeds Using Chemical Methods and an Amino Acid Analyzer
Falade, Olumuyiwa S.
Adewusi, Steve R. A.
JOURNAL OF AOAC INTERNATIONAL, 2013, 96 (01) : 102 - 109
[44] Anhydrides of amino acids and amino acid derivatives.
Karrer, P
Granacher, C
HELVETICA CHIMICA ACTA, 1924, 7 : 763 - 780
[45] SYNTHESIS OF AMINO ACIDS CATALYZED BY AMINO ACID OXIDASES
RADHAKRISHNAN, AN
MEISTER, A
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1957, 79 (21) : 5828 - 5829
[46] ANALYSIS OF NEUTRAL SUGARS AS GLYCAMINES USING AN AMINO-ACID ANALYZER
HARA, S
IKEGAMI, H
SHONO, A
MEGA, T
IKENAKA, T
MATSUSHIMA, Y
ANALYTICAL BIOCHEMISTRY, 1979, 97 (01) : 166 - 172
[47] PREDICTION OF LIMITING AMINO ACIDS IN 24 FOODS USING PLASMA AMINO ACID SCORE
MCLAUGHL.JM
NOEL, FJ
MORRISON, AB
RAO, SVK
FEDERATION PROCEEDINGS, 1966, 25 (2P1) : 541 - +
[48] DETERMINATION OF TAURINE IN FOODS AND FEEDS USING AN AMINO-ACID ANALYZER
ERBERSDOBLER, HF
GREULICH, HG
TRAUTWEIN, E
JOURNAL OF CHROMATOGRAPHY, 1983, 254 (JAN): : 332 - 334
[49] Synthesis of α-amino acids using amino acid γ-anion equivalents:: synthesis of 5-oxo α-amino acids, homophenylalanine derivatives and pentenylglycines
Jackson, RFW
Fraser, JL
Wishart, N
Porter, B
Wythes, MJ
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (12): : 1903 - 1912
[50] RAPID ESTIMATION OF DOPA IN PHYSIOLOGICAL FLUIDS USING AMINO ACID ANALYZER
HARE, TA
VOGEL, WH
BIOCHEMICAL MEDICINE, 1970, 4 (3-4): : 277 - &

← 1 2 3 4 5 →