Evaluation of hydrogen trapping in high strength steels by thermal desorption spectroscopy

被引:106
作者
Escobar, D. Perez [1 ]
Verbeken, K. [1 ,2 ]
Duprez, L. [3 ]
Verhaege, M. [1 ]
机构
[1] Univ Ghent, Dept Mat Sci & Engn, B-9052 Ghent, Belgium
[2] Max Planck Inst Eisenforsch GmbH, D-40237 Dusseldorf, Germany
[3] ArcelorMittal Res Ind Gent, B-9060 Zelzate, Belgium
来源
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 2012年 / 551卷
关键词
Austenite; Bainite; Martensite; Steel; Hydrogen embrittlement; DUAL-PHASE; DELAYED FRACTURE; IRON; EMBRITTLEMENT; BEHAVIOR; DAMAGE;
D O I
10.1016/j.msea.2012.04.078
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
High strength steels are materials of considerable interest and are increasingly used but appear to be more prone to hydrogen embrittlement (HE). In this work, four high strength steels and a pure iron, as a reference material, were studied by thermal desorption spectroscopy (TDS) in order to evaluate hydrogen trapping in these materials and to correlate it to the observed response of these materials to the previously evaluated effect of hydrogen on their mechanical properties. It was found that the materials which display a rather fast and significant ductility loss during hydrogen charged tensile testing contained a higher amount of diffusible hydrogen after charging. The activation energies for the peaks present in the TDS spectra were calculated for all materials and indicated that the activation energies for all low temperature peaks are pretty similar. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:50 / 58
页数:9
相关论文
共 42 条
  • [1] Barbe L., 2005, THESIS UGHENT
  • [2] Determination of Hydrogen in Steel by Thermal Desorption Mass Spectrometry
    Bergers, K.
    de Souza, E. Camisao
    Thomas, I.
    Mabho, N.
    Flock, J.
    [J]. STEEL RESEARCH INTERNATIONAL, 2010, 81 (07) : 499 - 507
  • [3] ROLE OF HYDROGEN IN EMBRITTLEMENT OF IRON AND STEEL
    BERNSTEI.IM
    [J]. MATERIALS SCIENCE AND ENGINEERING, 1970, 6 (01): : 1 - &
  • [4] Deformation behavior of low carbon TRIP sheet steels at high strain rates
    Choi, ID
    Bruce, DM
    Kim, SJ
    Lee, CG
    Park, SH
    Matlock, DK
    Speer, JG
    [J]. ISIJ INTERNATIONAL, 2002, 42 (12) : 1483 - 1489
  • [5] THERMAL-ANALYSIS OF TRAPPED HYDROGEN IN PURE IRON
    CHOO, WY
    LEE, JY
    [J]. METALLURGICAL TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1982, 13 (01): : 135 - 140
  • [6] Hydrogen degradation of high-strength weldable steels in seawater
    Cwiek, J
    Nikiforov, K
    [J]. MATERIALS SCIENCE, 2004, 40 (06) : 831 - 835
  • [7] ADSORPTION AND DIFFUSION OF ELECTROLYTIC HYDROGEIN IN PALLADIUM
    DEVANATHAN, MAV
    STACHURSKI, Z
    [J]. PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1962, 270 (1340): : 90 - &
  • [8] Duprez L., 2009, P INT HYDR C, P62
  • [9] Combined thermal desorption spectroscopy, differential scanning calorimetry, scanning electron microscopy and X-ray diffraction study of hydrogen trapping in cold deformed TRIP steel
    Escobar, D. Perez
    Depover, T.
    Duprez, L.
    Verbeken, K.
    Verhaege, M.
    [J]. ACTA MATERIALIA, 2012, 60 (6-7) : 2593 - 2605
  • [10] Internal and surface damage of multiphase steels and pure iron after electrochemical hydrogen charging
    Escobar, D. Perez
    Minambres, C.
    Duprez, L.
    Verbeken, K.
    Verhaege, M.
    [J]. CORROSION SCIENCE, 2011, 53 (10) : 3166 - 3176