Sodium dodecylsulfate induced synthesis of quinoxalines

被引:0
作者
Emmadi, Narender Reddy [1 ]
Atmakur, Krishnaiah [1 ]
机构
[1] CSIR, Indian Inst Chem Technol, Div Crop Protect Chem, Hyderabad 500007, Andhra Pradesh, India
来源
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | 2013年 / 52卷 / 12期
关键词
Phenacyl bromide; o-phenylene diamines; sodium dodecylsulfate (SDS); quinoxalines; EFFICIENT SYNTHESIS; MOLECULAR-IODINE; SOLVENT-FREE; WATER; CATALYST; DERIVATIVES; OXIDATION; PYRAZINES; PROTOCOL; POLYMER;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A simple and efficient sodium dodecylsulfate (SDS) induced method for the synthesis of quinoxalines in excellent yields in water at room temperature by the reaction of phenacyl bromide and o-phenylene diamines has been developed. Simple reaction conditions, wide compatibility and high yields are the advantages of this protocol.
引用
收藏
页码:1500 / 1504
页数:5
相关论文
共 26 条
[1]   Straightforward access to pyrazines, piperazinones, and quinoxalines by reactions of 1,2-diaza-1,3-butadienes with 1,2-diamines under solution, solvent-free, or solid-phase conditions [J].
Aparicio, Domitila ;
Attanasi, Orazio A. ;
Filippone, Paolino ;
Ignacio, Roberto ;
Lillini, Samuele ;
Mantellini, Fabio ;
Palacios, Francisco ;
Santos, Jesus M. de los .
JOURNAL OF ORGANIC CHEMISTRY, 2006, 71 (16) :5897-5905
[2]   Highly chemoselective addition of amines to epoxides in water [J].
Azizi, N ;
Saidi, MR .
ORGANIC LETTERS, 2005, 7 (17) :3649-3651
[3]  
Bailly C, 1999, ANTI-CANCER DRUG DES, V14, P291
[4]   An efficient protocol for the synthesis of quinoxaline derivatives at room temperature using molecular iodine as the catalyst [J].
Bhosale, RS ;
Sarda, SR ;
Ardhapure, SS ;
Jadhav, WN ;
Bhusare, SR ;
Pawar, RP .
TETRAHEDRON LETTERS, 2005, 46 (42) :7183-7186
[5]  
Brock E. D., 1999, [No title captured], Patent No. [WO 9951688, 9951688]
[6]  
Chakraborti AK, 2007, GREEN CHEM, V9, P1335, DOI 10.1039/b710414f
[7]   Catalyst-free chemoselective N-tert-butyloxycarbonylation of amines in water [J].
Chankeshwara, Sunay V. ;
Chakraborti, Asit K. .
ORGANIC LETTERS, 2006, 8 (15) :3259-3262
[8]  
Dailey S, 2001, J MATER CHEM, V11, P2238, DOI 10.1039/b104674h
[9]   An efficient and convenient protocol for the synthesis of quinoxalines and dihydropyrazines via cyclization-oxidation processes using HClO4•SiO2 as a heterogeneous recyclable catalyst [J].
Das, Biswanath ;
Venkateswarlu, Katta ;
Suneel, Kanaparthy ;
Majhi, Anjoy .
TETRAHEDRON LETTERS, 2007, 48 (31) :5371-5374
[10]   STRUCTURE REVISION OF ANTIBIOTIC ECHINOMYCIN [J].
DELL, A ;
WILLIAMS, DH ;
MORRIS, HR ;
SMITH, GA ;
FEENEY, J ;
ROBERTS, GCK .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (09) :2497-2502