Large Area Plan-View Transmission Electron Microscopy Sample Preparation for Multijunction Metamorphic Solar Cell Devices

被引:0
|
作者
Jackson, M. J. [1 ]
Jackson, B. L. [1 ]
Bodzin, N. [1 ]
Zakaira, A. [2 ]
Liu, X-Q. [2 ]
King, R. R. [2 ]
Goorsky, M. S. [1 ]
机构
[1] Univ Calif Los Angeles, Dept Mat Sci & Engn, Los Angeles, CA 90095 USA
[2] Spectrolab Inc, Sylmar, CA 91342 USA
来源
2012 38TH IEEE PHOTOVOLTAIC SPECIALISTS CONFERENCE (PVSC) | 2012年
关键词
Defect characterization; TEM; plan view; metamorphic devices; BUFFER LAYERS;
D O I
暂无
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
A focused ion beam (FIB) sample preparation technique is developed to produce very large areas of electron transparent material for plan-view transmission electron microscopy measurements from specific layers in a multi-layer device structure. An initial cross section FIB cut allows plan-view sample creation from any layer of interest, and therefore rapid characterization of the defect density as a function of depth is achievable for structures containing multiple layers, such as multi-junction metamorphic layer structures for high efficiency III-V solar cells. Uniform electron transparent plan-view areas of greater than 100 mu m(2) are extracted from a cross-section to facilitate observation of defect densities as low as similar to 10(6) cm(-2). To demonstrate the technique, the active cell layers of two inverted metamorphic III-V solar cell structures have been imaged to reveal defect densities as high as 109 cm-2 and as low as 10(6) cm(-2).
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页码:1620 / 1623
页数:4
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