1-Benzoyl-3-(6-methylpyridin-2-yl)thiourea

被引：3

作者：

Yusof, MSM

Soh, SKC

Ngah, N

Yamin, BM ^{[1
]}

机构：

[1] Univ Malaysia Terengganu, Dept Chem Sci, Fac Sci & Technol, Kuala Terengganu, Malaysia

[2] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷

关键词：

D O I：

10.1107/S1600536806009366

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The molecular structure of the title compound, C14H13N3OS, adopts a cis-trans configuration with respect to the positions of the benzoyl and 6-methylpyridin-2yl groups relative to the S atom across the thiourea C-N bonds. In the crystal structure, the molecules are linked by N-H center dot center dot center dot S, C-H center dot center dot center dot S and C-H center dot center dot center dot O interactions, forming a one-dimensional chain parallel to the b axis.

引用

页码：O1446 / O1448

页数：3

共 8 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS
ALLEN, FH
KENNARD, O
WATSON, DG
BRAMMER, L
ORPEN, AG
TAYLOR, R
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12): : S1 - S19
[2] *BRUK, 2000, SADABS VERS 2 01 SMA
[3] Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI [10.1107/S0021889895007138, DOI 10.1107/S0021889895007138]
[4] Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR
[5] SHELFO SW, 1997, ATLAS UROL CLIN N AM, V5, P1
[6] Single-crystal structure validation with the program PLATON
Spek, AL
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 : 7 - 13
[7] N′-benzoyl-N-p-bromophenylthiourea
Yamin, BM
Yusof, MSM
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O340 - O341
[8] N-Benzoyl-N′-phenylthiourea
Yamin, BM
Yusof, MSM
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2003, 59 : O151 - O152

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