1-Benzoyl-3-(6-methylpyridin-2-yl)thiourea

被引：3

作者：

Yusof, MSM

Soh, SKC

Ngah, N

Yamin, BM ^{[1
]}

机构：

[1] Univ Malaysia Terengganu, Dept Chem Sci, Fac Sci & Technol, Kuala Terengganu, Malaysia

[2] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷

关键词：

D O I：

10.1107/S1600536806009366

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The molecular structure of the title compound, C14H13N3OS, adopts a cis-trans configuration with respect to the positions of the benzoyl and 6-methylpyridin-2yl groups relative to the S atom across the thiourea C-N bonds. In the crystal structure, the molecules are linked by N-H center dot center dot center dot S, C-H center dot center dot center dot S and C-H center dot center dot center dot O interactions, forming a one-dimensional chain parallel to the b axis.

引用

页码：O1446 / O1448

页数：3

共 8 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2]

*BRUK, 2000, SADABS VERS 2 01 SMA

[3]

Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI [10.1107/S0021889895007138, DOI 10.1107/S0021889895007138]

[4]

Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR

[5]

SHELFO SW, 1997, ATLAS UROL CLIN N AM, V5, P1

[6] Single-crystal structure validation with the program PLATON [J].

Spek, AL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13

[7] N′-benzoyl-N-p-bromophenylthiourea [J].

Yamin, BM ;

Yusof, MSM .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 :O340-O341

[8] N-Benzoyl-N′-phenylthiourea [J].

Yamin, BM ;

Yusof, MSM .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2003, 59 :O151-O152

← 1 →