Demonstration of a chamber for strain mapping of steel specimens under mechanical load in a hydrogen environment by synchrotron radiation

被引:4
作者
Connolly, Matthew [1 ]
Park, Jun-Sang [2 ]
Bradley, Peter [1 ]
Lauria, Damian [1 ]
Slifka, Andrew [1 ]
Drexler, Elizabeth [1 ]
机构
[1] NIST, 325 Broadway, Boulder, CO 80305 USA
[2] Argonne Natl Lab, 9700 Cass Ave,Bldg 401, Lemont, IL 60439 USA
关键词
X-RAY-DIFFRACTION; DEFORMATION;
D O I
10.1063/1.5012541
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
We demonstrate a hydrogen gas chamber suitable for lattice strain measurements and capturing radiographs of a steel specimen under a mechanical load using high energy synchrotron x-rays. The chamber is suitable for static and cyclic mechanical loading. Experiments were conducted at the 1-ID-E end station of the Advanced Photon Source, Argonne National Laboratory. Diffraction patterns show a high signal-to-noise ratio suitable for lattice strain measurements for the specimen and with minimal scattering and overlap from the gas chamber manufactured from aluminum. In situ radiographs of a specimen in the hydrogen chamber show the ability to track a growing crack and to map the lattice strain around the crack with high spatial and strain resolution.
引用
收藏
页数:7
相关论文
共 17 条
[1]  
Almer J., ADV PHOTON SOURCE
[2]  
Chantler CT., 2005, X-ray form factor
[3]   Chamber for mechanical testing in H2 with observation by neutron scattering [J].
Connolly, Matthew ;
Bradley, Peter ;
Slifka, Andrew ;
Drexler, Elizabeth .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2017, 88 (06)
[4]   Elastoplastic deformation of ferritic steel and cementite studied by neutron diffraction and self-consistent modelling [J].
Daymond, MR ;
Priesmeyer, HG .
ACTA MATERIALIA, 2002, 50 (06) :1613-1626
[5]   High spatial resolution, high energy synchrotron x-ray diffraction characterization of residual strains and stresses in laser shock peened Inconel 718SPF alloy [J].
Gill, Amrinder S. ;
Zhou, Zhong ;
Lienert, Ulrich ;
Almer, Jonathan ;
Lahrman, David F. ;
Mannava, S. R. ;
Qian, Dong ;
Vasudevan, Vijay K. .
JOURNAL OF APPLIED PHYSICS, 2012, 111 (08)
[6]   The use of high energy X-rays from the Advanced Photon Source to study stresses in materials [J].
Haeffner, DR ;
Almer, JD ;
Lienert, U .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2005, 399 (1-2) :120-127
[7]   Neutron Imaging Detector With Scintillation Light Magnification And Amplification [J].
Hussey, D. S. ;
LaManna, J. M. ;
Baltic, E. ;
Jacobson, D. L. .
POLYMER ELECTROLYTE FUEL CELLS 16 (PEFC 16), 2016, 75 (14) :245-250
[8]  
Hutchings M. T., 2005, Introduction to the Characterization of Residual Stress by Neutron Diffraction
[9]  
Kaiser D.L., 2007, SRM 674b x-ray powder diffraction intensity set for quantitative analysis by x-ray powder diffraction
[10]   Experimental measurement of lattice strain pole figures using synchrotron x rays [J].
Miller, MP ;
Bernier, JV ;
Park, JS ;
Kazimirov, A .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2005, 76 (11) :1-11