共 49 条
Study on antibacterial activity of chemically synthesized PANI-Ag-Au nanocomposite
被引:51
作者:
Boomi, Pandi
[1
]
Prabu, Halliah Gurumallesh
[1
]
Manisankar, Paramasivam
[1
]
Ravikumar, Sundaram
[2
]
机构:
[1] Alagappa Univ, Sch Chem Sci, Dept Ind Chem, Karaikkudi 630003, Tamil Nadu, India
[2] Alagappa Univ, Dept Oceanog & Coastal Area Studies, Sch Marine Sci, Karaikkudi 623409, Tamil Nadu, India
关键词:
Polyaniline;
Chemical synthesis;
Composite materials;
Nanostructure;
Characterization;
Antibacterial activity;
GOLD NANOPARTICLES;
BIMETALLIC NANOPARTICLES;
SILVER NANOPARTICLES;
ELECTROCHEMICAL DEPOSITION;
STEP SYNTHESIS;
POLYANILINE;
STABILITY;
COMPOSITE;
PARTICLES;
OXIDE;
D O I:
10.1016/j.apsusc.2014.02.003
中图分类号:
O64 [物理化学(理论化学)、化学物理学];
学科分类号:
070304 ;
081704 ;
摘要:
Pristine polyaniline (PANI), PANI-Ag, PANI-Au and PANI-Ag-Au nanocomposites have been successfullysynthesized by chemical oxidative polymerization method using aniline as monomer, ammonium persulphate as oxidant and metal (Ag, Au and Ag-Au) colloids. UV-Vis analysis exhibited surface Plasmonresonances of Ag, Au, Ag-Au nanoparticles. FT-IR spectra revealed the shift in peak position of N-H stretching. X-ray diffraction (XRD) results confirm the presence of Ag, Au and Au-Ag nanoparticles. HR-TEMimages show nanosizes of Ag, Au, Ag-Au and the incorporation of such nanoparticles into the PANImatrix. Pristine PANI, PANI-Ag, PANI-Au and PANI-Ag-Au nanocomposites were tested for antibacterial activity by agar well diffusion method. PANI-Ag-Au nanocomposite exhibited higher antibacterialactivity against both gram-positive [Streptococcus sp. (MTCC 890), Staphylococcus sp. (MTCC 96)] andgramnegative bacteria [Escherichia coli (MTCC 1671) and Klebsiella sp. (MTCC 7407)] when comparedwith PANI-Ag nanocomposite, PANI-Au nanocomposite and pristine PANI. The novelty of this study is the polymerbimetal synthesis and its antibacterial potential. (C) 2014 Elsevier B.V. All rights reserved.
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页码:66 / 72
页数:7
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