Characterization and analysis of Semen Cuscutae by capillary gas chromatography and gas chromatography-mass spectrometry

被引：0
|
作者：
Li, Y
Ye, M
Liu, HW [1 ]
Ji, XH
Yan, YN
机构：
[1] Beijing Univ, Dept Chem, Beijing 100871, Peoples R China
[2] Beijing Univ Chinese Med, Beijing 100029, Peoples R China
来源：
JOURNAL OF SEPARATION SCIENCE | 2002年 / 25卷 / 04期
关键词：
capillary gas chromatography; gas chromatography-mass spectrometry; Semen Cuscutae; (+)-Sesamin; long chain fatty acids;
D O I：
10.1002/1615-9314(20020301)25:4<255::AID-JSSC255>3.0.CO;2-C
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Chloroform extracts of the Chinese herbal medicine Semen Cuscutae were analyzed by capillary gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS), and the pharmaceutically active component (+)-sesamin was identified and determined in this plant for the first time. Several n-alkanes, (+)-sesamin, and some compounds, identified by GC-MS and GC retention index, were chosen to characterize different samples of Semen Cuscutae. Fingerprints were obtained of the extracts of Semen Cuscutae from six sources. In addition, it was shown that some fatty acids are present in the seed oils (petroleum ether extracts) of Semen Cuscutae.
引用
收藏
页码：255 / 259
页数：5
相关论文
共 50 条
  • [31] Analysis of 28 insecticides in curry leaves (Murraya koenigii L.) by gas chromatography and gas chromatography-mass spectrometry
    Mohapatra, Soudamini
    Manikrao, Gourishankar
    Siddamallaiah, Lekha
    Buddidhathi, Radhika
    Mathada, Nagapooja Yogendraiah
    INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 2017, 97 (01) : 14 - 28
  • [32] Detection of Eltenac in the Horse: Identification of Phase I Metabolites in Urine by Capillary Gas Chromatography-Mass Spectrometry and the Determination of Excretion Profile by Liquid Chromatography-Mass Spectrometry
    M. C. Dumasia
    I. Morelli
    P. Teale
    Chromatographia, 2004, 59 : S115 - S121
  • [33] Detection of Eltenac in the horse: Identification of phase I metabolites in urine by capillary gas chromatography-mass spectrometry and the determination of excretion profile by liquid chromatography-mass spectrometry
    Dumasia, MC
    Morelli, I
    Teale, P
    CHROMATOGRAPHIA, 2004, 59 (Suppl 1) : S115 - S121
  • [34] Use of hydrogen as a carrier gas for the analysis of steroids with anabolic activity by gas chromatography-mass spectrometry
    Munoz-Guerra, J. A.
    Prado, P.
    Garcia-Tenorio, S. Vargas
    JOURNAL OF CHROMATOGRAPHY A, 2011, 1218 (41) : 7365 - 7370
  • [35] Determination of imidacloprid in vegetable samples by gas chromatography-mass spectrometry
    Navalon, A
    GonzalezCasado, A
    ElKhattabi, R
    Vilchez, JL
    FernandezAlba, AR
    ANALYST, 1997, 122 (06) : 579 - 581
  • [36] Quantification of clotiazepam in human plasma by gas chromatography-mass spectrometry
    Ahn, SH
    Maeng, HJ
    Koo, TS
    Kim, DD
    Shim, CK
    Chung, SJ
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2006, 834 (1-2): : 128 - 133
  • [37] Combination of TLC blotting and gas chromatography-mass spectrometry for analysis of peroxidized cholesterol
    Minami, Yuko
    Yokoi, Sayuri
    Setoyama, Mari
    Bando, Noriko
    Takeda, Sayaka
    Kawai, Yoshichika
    Terao, Junji
    LIPIDS, 2007, 42 (11) : 1055 - 1063
  • [38] Development of a gas chromatography-mass spectrometry method for the analysis of sitagliptin in human urine
    Ucakturk, Ebru
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2013, 74 : 71 - 76
  • [39] A simple approach to on-line oxidative pyrolysis-capillary gas chromatography-mass spectrometry
    Desmet, K
    Tienpont, B
    Schelfaut, M
    Sandra, P
    CHROMATOGRAPHIA, 2003, 57 (5-6) : 385 - 388
  • [40] Determination of triethanolamine in air samples by gas chromatography-mass spectrometry
    C. Giachetti
    Chromatographia, 1998, 48 : 443 - 449
12345