Characterization and analysis of Semen Cuscutae by capillary gas chromatography and gas chromatography-mass spectrometry

被引:0
|
作者
Li, Y
Ye, M
Liu, HW [1 ]
Ji, XH
Yan, YN
机构
[1] Beijing Univ, Dept Chem, Beijing 100871, Peoples R China
[2] Beijing Univ Chinese Med, Beijing 100029, Peoples R China
关键词
capillary gas chromatography; gas chromatography-mass spectrometry; Semen Cuscutae; (+)-Sesamin; long chain fatty acids;
D O I
10.1002/1615-9314(20020301)25:4<255::AID-JSSC255>3.0.CO;2-C
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Chloroform extracts of the Chinese herbal medicine Semen Cuscutae were analyzed by capillary gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS), and the pharmaceutically active component (+)-sesamin was identified and determined in this plant for the first time. Several n-alkanes, (+)-sesamin, and some compounds, identified by GC-MS and GC retention index, were chosen to characterize different samples of Semen Cuscutae. Fingerprints were obtained of the extracts of Semen Cuscutae from six sources. In addition, it was shown that some fatty acids are present in the seed oils (petroleum ether extracts) of Semen Cuscutae.
引用
收藏
页码:255 / 259
页数:5
相关论文
共 50 条
  • [1] Simultaneous profiling analysis of alkylphenols and amines by gas chromatography and gas chromatography-mass spectrometry
    Paik, MJ
    Choi, YM
    Kim, KR
    ANALYTICA CHIMICA ACTA, 2006, 560 (1-2) : 218 - 226
  • [2] Analysis of alkaloids in tobacco by gas chromatography-mass spectrometry
    Xu, YJ
    Bai, CM
    Zhong, KJ
    Huang, JG
    Tang, WY
    Lu, X
    Xu, GW
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2006, 34 (03) : 382 - 384
  • [3] Analysis of the volatile components in trogopterorum feces by capillary gas chromatography and gas chromatography/mass spectrometry
    Wei, Y
    Zhang, X
    Huang, AJ
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2001, 29 (02) : 195 - 198
  • [4] Determination of Acetochlor Residue in Food by Gas Chromatography and Gas Chromatography-Mass Spectrometry
    Dong Zhen-Lin
    Yang Chun-Guang
    Xiao Shan-Shan
    Zhao Jing-Hong
    Li Yi-Chen
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2009, 37 (05) : 698 - 702
  • [5] Analysis of phyto-oestrogens by gas chromatography-mass spectrometry
    Morton, M
    Arisaka, O
    Miyake, A
    Evans, B
    ENVIRONMENTAL TOXICOLOGY AND PHARMACOLOGY, 1999, 7 (03) : 221 - 225
  • [6] Application of Gas Chromatography-Mass Spectrometry to analysis Gasoline residues
    Liu, Shujun
    Zhao, Changzheng
    Yu, Lili
    ADVANCES IN CHEMICAL ENGINEERING, PTS 1-3, 2012, 396-398 : 2503 - 2506
  • [7] Analysis of Volatile Oil of Garlic by Gas Chromatography-Mass Spectrometry
    Guo Xiaofei
    Du Ailing
    Guan Congsheng
    Pan Guangmin
    Du Aiqin
    Wang Weiqiang
    CHINESE JOURNAL OF CHROMATOGRAPHY, 2005, 23 (05) : 548 - 550
  • [8] Gas chromatography-mass spectrometry analysis of pheomelanin degradation products
    Dernroth, Dzeneta Nezirevic
    Rundstrom, Annica
    Kagedal, Bertil
    JOURNAL OF CHROMATOGRAPHY A, 2009, 1216 (30) : 5730 - 5739
  • [9] Analysis of neutral nitromusks in incenses by capillary electrophoresis in organic solvents and gas chromatography-mass spectrometry
    Gotti, R
    Fiori, J
    Mancini, F
    Cavrini, V
    ELECTROPHORESIS, 2005, 26 (17) : 3325 - 3332
  • [10] Gas Chromatography-Differential Mobility Spectrometry and Gas Chromatography-Mass Spectrometry for the detection of coliform bacteria
    Saptalena, Lena Ganda
    Kuklya, Andriy
    Telgheder, Ursula
    INTERNATIONAL JOURNAL OF MASS SPECTROMETRY, 2015, 388 : 17 - 25