Separation of baicalin from Scutellaria Baicalensis Georgi with polyamide

被引:1
|
作者
Chi Ru-an [1 ,2 ]
Zhou Fang [1 ,2 ]
Huang Kun [1 ]
Zhang Yue-fei [1 ]
机构
[1] Wuhan Inst Technol, Sch Chem Engn & Pharm, Wuhan 430073, Peoples R China
[2] Wuhan Inst Technol, Minist Educ, Key Lab Green Chem Proc, Wuhan 430073, Peoples R China
来源
关键词
baicalin; Scutellaria Baicalensis Georgi; adsorption; separation;
D O I
10.1007/s11771-008-0113-9
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
Separation of baicalin from Scutellaria Baicalensis Georgi with polyamide was studied. The adsorption isotherm, kinetic equation and desorption law were investigated by static and dynamic adsorption methods. The results show that the kinetic behavior is mainly controlled by the liquid film diffusion process and obeys the Boyd film diffusion equation. Equilibrium data for the adsorption of baicalin are correlated with Freundlich isotherm equation, i.e. q=3.8c(e)(2.057), suggesting that the relative capacity of polyamide to baicalin is somewhat small. The desorption results indicate that the baicalin with mass fraction of 33.86% and the least impurities can be obtained by chromatography using 60% ethanol as the eluant at room temperature.
引用
收藏
页码:606 / 611
页数:6
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