A new facile synthesis of ultra fine magnesium oxide nanowires and optical properties

被引:36
作者
Al-Ghamdi, Ahmed A. [1 ]
Al-Hazmi, Faten [1 ]
Alnowaiser, Fowzia [2 ]
Al-Tuwirqi, Reem M. [1 ]
Al-Ghamdi, Attieh A. [1 ]
Alhartomy, Omar A. [1 ]
El-Tantawy, Farid [3 ]
Yakuphanoglu, F. [1 ,4 ]
机构
[1] King Abdulaziz Univ, Dept Phys, Fac Sci, Jeddah 21589, Saudi Arabia
[2] King Abdulaziz Univ, Dept Chem, Fac Sci, Jeddah 21589, Saudi Arabia
[3] Suez Canal Univ, Dept Phys, Fac Sci, Ismailia, Egypt
[4] Firat Univ, Dept Phys, Fac Sci, TR-23169 Elazig, Turkey
关键词
nanostructures; chemical synthesis; optical properties; LASER-ABLATION; MGO; NANOPARTICLES;
D O I
10.1007/s10832-012-9761-0
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
One-dimensional metal oxides nanowires like magnesium oxide (MgO) play an important role in several nanotechnological applications. MgO nanowires were synthesized for the first time via hydrothermal route using magnesium acetate and urea at 180 A degrees C for 2 h. The synthesized MgO nanowires were characterized by means of X-ray diffraction (XRD), Fourier transformer Infrared spectroscopy (FTIR), field emission scanning electron microscopy (FESEM), energy dispersive X-ray spectroscopy (EDS), transmission scanning electron microscopy (TEM) and thermal gravimetric analysis (TGA). The obtained results indicated that the MgO nanowires show a predominant well- crystalline cubic face-centered with an average diameter of 10 nm and an average length of 40 mu m. The optical band gap energy of the sample was found to be 3.45 eV. The sample indicates a broadband PL emission in UV region and exhibits a good photoluminescence behavior for photonic devices applications. It is evaluated that this novel synthetic method is very useful and serves as a facile, direct preparation mild chemical method giving mass production of one dimensional MgO nanowires.
引用
收藏
页码:198 / 203
页数:6
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