Structural, morphological and magnetic properties of NiFe2O4 nano-particles

被引：137

作者：

Alarifi, A. ^{[1
]}

Deraz, N. M. ^{[1
,2
]}

Shaban, S. ^{[3
]}

机构：

[1] King Saud Univ, Coll Sci, Dept Chem, Riyadh 11451, Saudi Arabia

[2] Natl Res Ctr, Dept Phys Chem, Lab Surface Chem & Catalysis, Cairo, Egypt

[3] EPRI, Refining Div, Nasr City, Cairo, Egypt

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2009年 / 486卷 / 1-2期

关键词：

IR; SEM; TEM; M-s; Hc; Density; Crystallite size; Ni-ferrite; NICKEL FERRITE; CATION DISTRIBUTION; SPIN DISORDER; NANOPARTICLES; DECOMPOSITION; TEMPERATURE; BEHAVIOR; COBALT; COPPER; PURE;

D O I：

10.1016/j.jallcom.2009.06.192

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

NiFe2O4 nano-particles were synthesized by a simple and cost-effective method using Ni and Fe nitrates and glycine. Significant effect of the ratio between glycine and nitrates on the physical parameters like crystalline phase, crystallite size, and particle size, lattice constant and magnetic properties of the nano-particles has been investigated. The X-ray diffraction, IR and selected-area electron diffraction results indicated that the synthesized nickel ferrite particles have the nanometer size and inverse spinel structure. Room temperature magnetization results showed a ferromagnetic behavior of the NiFe2O4 nano-particles, with saturation specific magnetization values in the range of 2.387-57 emu/g at 15 kOe. The corecivity of the NiFe2O4 nano-powders changed from 65.58 to 148.8 Oe according to the change in the ratio between glycine and nitrates. (C) 2009 Elsevier B.V. All rights reserved.

引用

页码：501 / 506

页数：6

共 44 条

[1]

[Anonymous], PHYS MAGNETISM

[2] EFFECT OF HYDROTHERMAL SYNTHESIS ENVIRONMENT ON THE PARTICLE MORPHOLOGY, CHEMISTRY AND MAGNETIC-PROPERTIES OF BARIUM HEXAFERRITE [J].

ATAIE, A ;

PIRAMOON, MR ;

HARRIS, IR ;

PONTON, CB .

JOURNAL OF MATERIALS SCIENCE, 1995, 30 (22) :5600-5606

[3] Structural and electrical properties of Nil-xMgxFe2O4 synthesized by citrate gel process [J].

Berchmans, LJ ;

Selvan, RK ;

Kumar, PNS ;

Augustin, CO .

JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2004, 279 (01) :103-110

[4] Temperature dependence of superparamagnetic resonance of iron oxide nanoparticles [J].

Berger, R ;

Bissey, JC ;

Kliava, J ;

Daubric, H ;

Estournès, C .

JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2001, 234 (03) :535-544

[5] Microstructure characterization of mechanosynthesized nano crystalline NiFe2O4 by Rietveld's analysis [J].

Bid, S. ;

Sahu, P. ;

Pradhan, S. K. .

PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES, 2007, 39 (02) :175-184

[6] Size-dependent magnetic properties of MnFe2O4 fine particles synthesized by coprecipitation [J].

Chen, JP ;

Sorensen, CM ;

Klabunde, KJ ;

Hadjipanayis, GC ;

Devlin, E ;

Kostikas, A .

PHYSICAL REVIEW B, 1996, 54 (13) :9288-9296

[7] Magnetic properties of nanostructured ferrimagnetic zinc ferrite [J].

Chinnasamy, CN ;

Narayanasamy, A ;

Ponpandian, N ;

Chattopadhyay, K ;

Guérault, H ;

Greneche, JM .

JOURNAL OF PHYSICS-CONDENSED MATTER, 2000, 12 (35) :7795-7805

[8]

Cullity B.D., 1972, INTRO MAGNETIC MAT

[9]

CULLITY BD, 1976, ELEMENTS XRAY DIFFRA, pCH4

[10] THE OBSERVATION OF MULTIAXIAL ANISOTROPY IN ULTRAFINE COBALT FERRITE PARTICLES USED IN MAGNETIC FLUIDS [J].

DAVIES, KJ ;

WELLS, S ;

UPADHYAY, RV ;

CHARLES, SW ;

OGRADY, K ;

ELHILO, M ;

MEAZ, T ;

MORUP, S .

JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 1995, 149 (1-2) :14-18

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