Ammonium Oxalate as an Efficient Catalyst for One-Pot Synthesis of Tetrahydrobenzo [a]xanthen-11-one Derivatives Under Solvent-Free Conditions

被引：4

作者：

Esfahani, Hamid R. M. ^{[1
]}

Foroughifar, Naser ^{[1
]}

Mobinikhaledi, Akbar ^{[2
]}

Moghanian, Hassan ^{[3
]}

机构：

[1] Islamic Azad Univ, Dept Chem, Tehran North Branch, Tehran, Iran

[2] Arak Univ, Dept Chem, Fac Sci, Arak, Iran

[3] Islamic Azad Univ, Dezful Branch, Dezful, Iran

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2013年 / 43卷 / 06期

关键词：

ammonium oxalate; multicomponent; one-pot; solvent-free; xanthene; BETA-NAPHTHOL; CONDENSATION; ALDEHYDES;

D O I：

10.1080/15533174.2012.754767

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A simple and efficient procedure for the synthesis of 12-aryl- or 12-alkyl-8,9,10,12-tetrahydrobenzo[a]xanthen-11-one derivatives has been developed via one-pot three-component reaction of 2-naphthol, aldehydes, and dimedone in the presence of ammonium oxalate as a mild and inexpensive catalyst under solvent-free conditions. The present method is operationally simple and offers several advantages such as high yields, short reaction time, economic availability of the catalyst, and simple workup.

引用

页码：752 / 755

页数：4

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