Novel two-component supramolecular association mode between carboxylic acids realized in the crystalline complex of 1,1′-binaphthyl-2,2′-dicarboxylic acid and formic acid

被引：1
作者：
Ibragimov, BT
Beketov, KM
Makhkamov, KK
Weber, E
机构：
[1] Uzbekistan Acad Sci, Inst Bioorgan Chem, Tashkent 700143, Uzbekistan
[2] Tech Univ Bergakad, Inst Organ Chem, D-09596 Freiberg, Germany
来源：
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY | 1999年 / 34卷 / 01期
关键词：
X-ray crystallography; H-bond; host-guest complex; supramolecular associate; catenated structure;
D O I：
10.1023/A:1008031123818
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A novel type of two-component H-bonded supramolecular associate (21-membered pseudo-macrocyclic rings) formed between mono- and dicarboxylic acids is found in the crystalline complex of 1,1'-binaphthyl-2,2'-dicarboxylic acid and formic acid. The crystal data are: (C22H14O4).(CH2O2), a = 12.904(3) Angstrom, b = 8.829(2) Angstrom, c = 33.348(2) Angstrom, V = 3799(2) Angstrom(3), orthorhombic, Pbca, Z = 8, R = 0.060 (F > 4 sigma), 2649 reflections.
引用
收藏
页码：31 / 37
页数：7
相关论文
共 20 条
[1]  
[Anonymous], 1995, ANGEW CHEM, V107, P2541
[2]  
Bernstein J., 1995, ANGEW CHEM, V107, P1689
[3]   VERSATILITY OF THE 1,1'-BINAPHTHYL-2,2'-DICARBOXYLIC ACID HOST IN SOLID-STATE INCLUSION - CRYSTAL AND MOLECULAR-STRUCTURES OF THE DIMETHYLFORMAMIDE (1-2), DIMETHYLSULFOXIDE (1-1), AND BROMOBENZENE (1-1) CLATHRATES [J].
CSOREGH, I ;
SJOGREN, A ;
CZUGLER, M ;
CSERZO, M ;
WEBER, E .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1986, (04) :507-513
[4]   THE UNUSUAL STRUCTURE OF THE CRYSTALLINE INCLUSION COMPOUND BETWEEN (11S,12S)-(-)-9,10-DIHYDRO-9,10-ETHANOANTHRACENE-11,12-DICARBOXYLIC ACID AND ACETIC-ACID [J].
CSOREGH, I ;
GALLARDO, O ;
WEBER, E ;
FINGE, S ;
REUTEL, C .
TETRAHEDRON-ASYMMETRY, 1992, 3 (12) :1555-1562
[5]   FORMATION OF ISOLATED GUEST DIMERS VS HOST GUEST COORDINATION - X-RAY CRYSTAL-STRUCTURES OF 4 CARBOXYLIC-ACID INCLUSION-COMPOUNDS FORMED BY ROOF-SHAPED AND SCISSOR-LIKE HOST MOLECULES [J].
CSOREGH, I ;
CZUGLER, M ;
WEBER, E ;
AHRENDT, J .
JOURNAL OF INCLUSION PHENOMENA AND MOLECULAR RECOGNITION IN CHEMISTRY, 1990, 8 (03) :309-322
[6]   SELECTIVE CLATHRATE FORMATION WITH THE NEW HOST SYSTEMS CIS AND TRANS-9,10-DIHYDRO-9,10-ETHANOANTHRACENE-11,12-DICARBOXYLIC ACID - INCLUSION PROPERTIES AND X-RAY STRUCTURE OF AN ENCAPSULATED ACETIC-ACID DIMER [J].
CZUGLER, M ;
WEBER, E ;
AHRENDT, J .
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (24) :1632-1634
[7]  
Desiraju G.R., 1996, CRYSTAL SUPRAMOLECUL, V2
[8]   Self-assembly of a two-component hydrogen-bonded network: Comparison of the two-dimensional structure observed by scanning tunneling microscopy and the three-dimensional crystal lattice [J].
EichhorstGerner, K ;
Stabel, A ;
Moessner, G ;
Declerq, D ;
Valiyaveettil, S ;
Enkelmann, V ;
Mullen, K ;
Rabe, JP .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1996, 35 (13-14) :1492-1495
[9]  
EICHHORSTGERNER K, 1996, ANGEW CHEM, V108, P1599
[10]   Polymorphism of crystalline host-guest complexes and unsolvated hosts .6. Pseudo-dimorphism of complexes between 1,1'-binaphthyl-2,2'-dicarboxylic acid and ethanol. X-ray crystal structures of the beta-form and of the unsolvated host compound [J].
Ibragimov, B ;
Beketov, K ;
Makhkamov, K ;
Weber, E .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1997, (07) :1349-1352
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