High frequency permeability of Fe-Cu-Nb-Si-B nanocrystalline flakes with the distribution of shape anisotropy fields

Fe-Cu-Nb-Si-B flakes with multiphase nanostructures have been obtained by annealing the amorphous ribbon and subsequently ball milled for 30 h. The crystal structures have been examined by X-ray diffraction pattern and Mossbauer spectrum. The results show that the particles annealed at 900 degrees C are made up of amorphous ferromagnetic phase, alpha-Fe3Si ferromagnetic phase and Fe2B phase, and the average hyperfine magnetic field (H-Bhf) of particles is 24.02 T. Meanwhile, the relationships between the structure and the high frequency permeability have been studied. Compared with particles annealed at 600 degrees C, particles annealed at 900 degrees C exhibit higher saturation magnetization, which is evidenced by the larger H-Bhf. Also, three magnetic loss peaks in a permeability spectrum have been observed for the particles annealed at 900 degrees C. The natural resonance frequencies are calculated, which are in good agreement with the experimental resonance peaks. The origin of the multiple magnetic loss peaks can be explained from the perspective of the distribution of shape anisotropy fields which is caused by multiple phase structure. (C) 2017 Elsevier B.V. All rights reserved.