Enzymatic preparation of structured TAG containing conjugated linoleic acid (CLA) at solvent-free

被引:8
作者
Yu, Dianyu [2 ]
Chen, Jun [2 ]
Cheng, Jie [2 ]
Chen, Yan [2 ]
Jiang, Lianzhou [2 ]
Qin, Lanxia [2 ]
Wang, Liqi [1 ]
机构
[1] Harbin Univ Commerce, Sch Comp & Informat Engn, Harbin 150028, Peoples R China
[2] Northeast Agr Univ, Sch Food Sci, Harbin 150030, Peoples R China
关键词
conjugated linoleic acid; lipid compounds; refrigerated centrifugation; supercritical CO2; RICE BRAN OIL; VEGETABLE-OILS; SOYBEAN OIL; FAT; TRANSESTERIFICATION; REESTERIFICATION; OPTIMIZATION; CRUDE;
D O I
10.1515/ijfe-2020-0023
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
Rice bran oil extracted by the water-enzymatic method was placed at a temperature of -5 degrees C for 8 h. Light-phase rice bran oil with an iodine value of 112.13 +/- 0.21 g I-2/100 g oil was separated by cryogenic freezing centrifugation. Lipozyme RM IM transesterified light-phase rice bran oil and conjugated linoleic acid (CLA) under supercritical system CO2 (SC-CO2). The optimal reaction conditions for transesterification of CLA and rice bran oil in SC-CO2 were determined as follows: the Lipozyme RM IM dosage was 9%, and the RBO/CLA molar ratio was 1:3, the reaction temperature was 55 degrees C, stirring speed was 300 rpm, and transesterification time was 20 h, the CLA conversion rate can reach 42.1%.
引用
收藏
页数:8
相关论文
共 29 条
  • [1] Enzymatic Production of Trans-Free Hard Fat Stock from Fractionated Rice Bran Oil, Fully Hydrogenated Soybean Oil, and Conjugated Linoleic Acid
    Adhikari, P.
    Shin, J. -A.
    Lee, J. -H.
    Hu, J. -N.
    Hwang, K. T.
    Lee, K. -T.
    [J]. JOURNAL OF FOOD SCIENCE, 2009, 74 (02) : E87 - E96
  • [2] Enzymatic transesterification of fractionated rice bran oil with conjugated linoleic acid: Optimization by response surface methodology
    Alim, M. A.
    Lee, J. -H.
    Akoh, C. C.
    Choi, M. -S.
    Jeon, M. -S.
    Shin, J. -A.
    Lee, K. -T.
    [J]. LWT-FOOD SCIENCE AND TECHNOLOGY, 2008, 41 (05) : 764 - 770
  • [3] Effect of method of stabilization on aqueous extraction of rice bran oil
    Amarasinghe, B. M. W. P. K.
    Kumarasiri, M. P. M.
    Gangodavilage, N. C.
    [J]. FOOD AND BIOPRODUCTS PROCESSING, 2009, 87 (C2) : 108 - 114
  • [4] AOCS, 1997, OFF METH REC PRACT A
  • [5] Processing of commercial rice bran for the production of fat and nutraceutical rich rice brokens, rice germ and pure bran
    Bhatnagar, A. S.
    Prabhakar, D. S.
    Kumar, P. K. Prasanth
    Rajan, R. G. Raja
    Krishna, A. G. Gopala
    [J]. LWT-FOOD SCIENCE AND TECHNOLOGY, 2014, 58 (01) : 306 - 311
  • [6] Chen J, 2017, RSC ADV, V7, P547
  • [7] A rapid procedure for analysing rice bran tocopherol, tocotrienol and γ-oryzanol contents
    Chen, MH
    Bergman, CJ
    [J]. JOURNAL OF FOOD COMPOSITION AND ANALYSIS, 2005, 18 (2-3) : 139 - 151
  • [8] Optimization and oxidative stability of biodiesel production from rice bran oil
    El Boulifi, N.
    Bouaid, A.
    Martinez, M.
    Aracil, J.
    [J]. RENEWABLE ENERGY, 2013, 53 : 141 - 147
  • [9] Investigation of the Immunomodulatory Potential of Oryzanol Isolated from Crude Rice Bran Oil in Experimental Animal Models
    Ghatak, Somsuvra B.
    Panchal, Shital J.
    [J]. PHYTOTHERAPY RESEARCH, 2012, 26 (11) : 1701 - 1708
  • [10] Conjugated linoleic acid (CLA) production and lipasecatalyzed interesterification of purified CLA with canola oil
    Goli, Sayyed Amir Hossein
    Kadivar, Mahdi
    Keramat, Javad
    Fazilati, Mohammad
    [J]. EUROPEAN JOURNAL OF LIPID SCIENCE AND TECHNOLOGY, 2008, 110 (05) : 400 - 404