One-step synthesis of conductive ceria/polypyrrole nanocomposite particles via photo-induced polymerization method

被引：12
作者：
Heydarnezhad, Hamid Reza [1 ]
Pourabbas, Behzad [1 ]
机构：
[1] Sahand Univ Technol, Dept Polymer Engn, Nanostruct Mat Res Ctr, Tabriz 513351996, Iran
来源：
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS | 2013年 / 24卷 / 11期
关键词：
CORE-SHELL NANOPARTICLES; VIBRATIONAL-SPECTRA; ANILINE DERIVATIVES; DOPED POLYPYRROLE; ELECTRON-TRANSFER; LATTICE-DYNAMICS; IMAGE-FORMATION; PHOTOPOLYMERIZATION; PYRROLE; COMPLEX;
D O I：
10.1007/s10854-013-1413-x
中图分类号：
TM [电工技术]; TN [电子技术、通信技术];
学科分类号：
0808 ; 0809 ;
摘要：
Inorganic-organic nanocomposites of ceria/polypyrrole with core/shell morphology and median diameter about of 150 nm in single nanoparticles were synthesized by a novel one-step photo-polymerization method using cerium (III) nitrate hexahydrate dissolved in acetonitrile and irradiation under UV wavelengths for 2 h. The photo-polymerization products were characterized using high resolution transmission electron microscopy, Fourier-transform infrared spectroscopy, energy-dispersive X-ray spectroscopy, wide-angle X-ray diffraction, particle size analysis, and field emission scanning electron microscope. Crystalline/amorphous structure was detected for the obtained core/shell nanoparticles via selected area electron diffraction pattern. Electrical conductivity of the nanoparticles was measured by four-probe technique.
引用
收藏
页码：4378 / 4385
页数：8
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