2,2-Dimethyl-5-[(4-methylthiazol-2-ylamino)methylene]-1,3-dioxane-4,6-dione

被引：0
作者：
da Silva, LE
Joussef, AC
Andrighetti-Fröhner, CR
Simoes, CMO
Bortoluzzi, AJ [1 ]
机构：
[1] Univ Fed Santa Catarina, Dept Quim, BR-88040900 Florianopolis, SC, Brazil
[2] Tech Univ Darmstadt, Clemens Schopf Inst Organ Chem & Biochem, D-64287 Darmstadt, Germany
[3] Univ Fed Santa Catarina, Dept Ciencias Farmaceut, BR-88040900 Florianopolis, SC, Brazil
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷
关键词：
D O I：
10.1107/S1600536806006064
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C11H12N2O4S, the thiazole ring is nearly planar. The 1,3-dioxane-4,6-dione ring exhibits a half-chair conformation. The NH group forms an intramolecular contact to a carbonyl O atom, forming a six-membered ring, and an intermolecular N-H center dot center dot center dot O hydrogen bond, with an H center dot center dot center dot O distance of 2.16 angstrom, is also observed.
引用
收藏
页码：O1163 / O1164
页数：2
相关论文
共 50 条
[21]   5-[(6-Fluoro-1,3-benzothiazol-2-ylamino)-methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione [J].
da Silva, LE ;
Joussef, AC ;
Foro, S ;
Schmidt, B .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O742-O743
[22]   5-[(4-Methoxyphenylamino) methylene]2,2-dimethyl-1,3-dioxane-4,6-dione [J].
da Silva, LE ;
Joussef, AC ;
Nunes, RJ ;
Andrighetti-Fröhner, CR ;
Bortoluzzi, AJ .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O4121-O4122
[23]   5-[(2-bromophenylamino)methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione [J].
da Silva, LE ;
Joussef, AC ;
Nunes, RJ ;
Andrighetti-Fröhner, CR ;
Bortoluzzi, AJ .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O4252-O4253
[24]   2,2-dimethyl-5-(4H-1,2,4-triazol-4-ylaminomethylene)-1,3-dioxane-4,6-dione monohydrate [J].
Joussef, AC ;
da Silva, LE ;
Bortoluzzi, AJ ;
Foro, S .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O2642-O2643
[25]   2,2-DIMETHYL-5-(2-METHYL-4-PHENYL-3,4-DIAZA-2-BUTENYLIDENE)-1,3-DIOXANE-4,6-DIONE [J].
BLAKE, AJ ;
MCNAB, H .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1995, 51 (51) :527-529
[26]   5-(anilinomethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione [J].
Vencato, Ivo ;
Cunha, Silvio ;
Ferrari, Jailton ;
Sabino, Jose R. .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O4062-O4064
[27]   5-(aminomethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione [J].
da Silva, Luiz Everson ;
Joussef, Antonio Carlos ;
Silva, Luciano Luiz ;
Foro, Sabine ;
Schmidt, Boris .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O3866-O3867
[28]   STRUCTURE OF 2,2-DIMETHYL-5-METHYLAMINOMETHYLENE-1,3-DIOXANE-4,6-DIONE [J].
DIANEZ, MJ ;
LOPEZCASTRO, A .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1991, 47 :1028-1030
[29]   2,2-DIMETHYL-5-(5-R-FURFURYLYDENE-2)-1,3-DIOXANE-4,6-DIONES .3. CRYSTAL AND MOLECULAR-STRUCTURE OF 2,2-DIMETHYL-5-(5-METHYL-2-FURFURYLYDENE)-1,3-DIOXANE-4,6-DIONE [J].
KRAPIVIN, GD ;
ZAVODNIK, VE ;
BELSKII, VK ;
VALTER, NI ;
KULNEVICH, VG .
KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1988, (11) :1453-1456
[30]   5-(4-Chloroanilinomethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione [J].
Yang, Jin-Cheng ;
Shi, Jian-You ;
Luo, You-Fu ;
Qiu, Neng ;
Chen, Li-Juan .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :01706-U3544
12345