Analysis of Volatile Compounds in Different Parts of Panax Quinquefolius L. by Online Gel Permeation Chromatography-Gas Chromatography/Mass Spectrometry System

被引：0
作者：
Ping, Hua [1 ,2 ]
Wang, Jihua [1 ,2 ]
Ma, Zhihong [1 ]
Lu, Anxiang [1 ]
Shu, Xiuli [1 ]
Pan, Ligang [1 ]
机构：
[1] Beijing Res Ctr Agrifood Testing & Farmland Monit, Beijing 100097, Peoples R China
[2] Natl Engn Res Ctr Informat Technol Agr, Beijing 100097, Peoples R China
来源：
SENSOR LETTERS | 2012年 / 10卷 / 1-2期
关键词：
American Ginseng; Accelerated Solvent Extraction; Volatile Compounds; Gel Permeation Chromatography-Gas Chromatography/Mass Spectrometry; CONJUGATED LINOLEIC-ACID; MASS-SPECTROMETRY; SOLVENT-EXTRACTION; GINSENG; GINSENOSIDES; PESTICIDES; ROOTS; AGES; OILS;
D O I：
10.1166/sl.2012.1833
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
An online gel permeation chromatography-gas chromatography/mass spectrometry (GPC-GC/MS) method was developed for determining volatile compounds in different parts of Panax quinquefolius L. (American ginseng). First, samples were extracted by accelerated solvent extraction (ASE), and the optimum ASE operations were dichloromethane as extraction solvent, 100 degrees C of extraction temperature and 7 min of static extraction time. Then the compounds with important bioactivities were purified, isolated and monitored by online GPC-GC/MS system. In total, twenty four volatile compounds were characterized in the four parts (root, stem, leaf and flower) of American ginseng. The main components in root and stem were 10,12-Octadecadienoic acid and Falcarinol, respectively; for leaf and flower, 9,12-Octadecadienoic acid was the major component. It was indicated that the combination of ASE technique and online GPC-GC/MS system was a rapid extraction, purification, determination and characterization of volatile compounds in root, stem, leaf and flower of American ginseng.
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页码：619 / 624
页数：6
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