Rapid and precise preparation of reactive benzeneselenolate solutions by reduction of diphenyl diselenide with hydrazine-sodium methanolate

被引：16

作者：

Henriksen, L ^{[1
]}

Stuhr-Hansen, N ^{[1
]}

机构：

[1] Univ Copenhagen, Dept Chem, DK-2100 Copenhagen, Denmark

来源：

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1 | 1999年 / 14期

关键词：

D O I：

10.1039/a903686e

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Solutions of sodium benzeneselenolate sufficiently reactive to effect aromatic substitution and;ester dealkylation are prepared in DMSO or NMP from diphenyl diselenide and hydrazine hydrate by titration with. methanolic;sodium methanolate.

引用

页码：1915 / 1916

页数：2

共 14 条

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