A Comparison on Physical, Structural, and Photocatalytical Properties of TiO2 Nanopowders Produced Using Sol-Gel and Flame Spray Pyrolysis

被引:14
作者
Erol, Mustafa [1 ,2 ,3 ]
Sancakoglu, Orkut [1 ,2 ]
Yurddaskal, Metin [1 ,2 ,4 ]
Yildirim, Serdar [1 ,2 ]
Celik, Erdal [1 ,5 ]
机构
[1] Dokuz Eylul Univ, Dept Met & Mat Engn, TR-35160 Izmir, Turkey
[2] Dokuz Eylul Univ, Grad Sch Nat & Appl Sci, TR-35160 Izmir, Turkey
[3] Hitit Univ, Dept Met & Mat Engn, TR-19000 Corum, Turkey
[4] Afyon Kocatepe Univ, Dept Met & Mat Engn, TR-03200 Afyon, Turkey
[5] Dokuz Eylul Univ, Ctr Prod & Applicat Elect Mat, TR-35160 Izmir, Turkey
关键词
WATER; IRRADIATION; DEGRADATION; OXIDATION; SURFACE;
D O I
10.1111/ijac.12018
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this study, nanoscale photocatalyst TiO2 powders were synthesized via sol-gel and flame spray pyrolysis (FSP). Phase structures and ratios were analyzed by X-ray diffractometer (XRD). Size, specific surface area, and morphologies were determined using particle size analyzer, Brunauer-Emmett-Teller theory, and scanning electron microscope, respectively. Anatase phase with some rutile together was obtained in XRD analysis. The degradation rates of aqueous methylene blue (MB) by TiO2 nanopowders were calculated using UV-vis spectrophotometer. It was found that MB decomposition was successfully achieved with significantly high efficiencies for both sol-gel and FSP-derived powders with small differences.
引用
收藏
页码:931 / 938
页数:8
相关论文
共 19 条
[1]  
[Anonymous], THESIS U NEW S WALES
[2]  
[Anonymous], DESALINATION
[3]   Al2O3-TiO2 thin films on glass substrate by sol-gel technique [J].
Celik, Erdal ;
Keskin, Ibrahim ;
Kayatekin, Isil ;
Azem, Funda Ak ;
Ozkan, Erhan .
MATERIALS CHARACTERIZATION, 2007, 58 (04) :349-357
[4]   Preparation and characterization of CeO2/TiO2 nanoparticles by flame spray pyrolysis [J].
Chaisuk, Choowong ;
Wehatoranawee, Anusara ;
Preampiyawat, Sirichai ;
Netiphat, Sirirat ;
Shotipruk, Artiwan ;
Panpranot, Joongjai ;
Jongsomjit, Banjerd ;
Mekasuwandumrong, Okorn .
CERAMICS INTERNATIONAL, 2011, 37 (05) :1459-1463
[5]   Synthesis and photocatalytic behaviors of Cr2O3-CNT/TiO2 composite materials under visible light [J].
Chen, Ming Liang ;
Cho, Kwang Youn ;
Oh, Won Chun .
JOURNAL OF MATERIALS SCIENCE, 2010, 45 (24) :6611-6616
[6]  
Ertl G., 1999, Preparation of Solid Catalysts
[7]  
Ertl G., 1997, HDB HETEROGENEOUS CA, V1-5
[8]   Preface [J].
Fan, Yuhong ;
Fisher, George ;
Leibacher, John .
SOLAR PHYSICS, 2012, 277 (01) :1-2
[9]   Heterogeneous photocatalytic oxidation of cyprodinil and fludioxonil in leaching water under solar irradiation [J].
Fenoll, Jose ;
Ruiz, Encarnacion ;
Hellin, Pilar ;
Flores, Pilar ;
Navarro, Simon .
CHEMOSPHERE, 2011, 85 (08) :1262-1268
[10]   Nanosized TiO2 Photocatalyst Powder via Sol-Gel Method: Effect of Hydrolysis Degree on Powder Properties [J].
Hafizah, Nor ;
Sopyan, I. .
INTERNATIONAL JOURNAL OF PHOTOENERGY, 2009, 2009