Determination of Neutral Saccharides by Capillary Electrophoresis with Contactless Conductivity Detection

被引:0
作者
Malkova, Klara [1 ]
Samcova, Eva [1 ]
Tuma, Petr [1 ]
机构
[1] Charles Univ Prague, Fac Med 3, Inst Biochem Cell & Mol Biol, Prague 10000 10, Czech Republic
来源
MODERN ELECTROCHEMICAL METHODS XXXI | 2011年
关键词
Capillary electrophoresis; Contactless conductivity detection; Saccharides; ZONE-ELECTROPHORESIS; UV DETECTION;
D O I
暂无
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
Capillary electrophoresis with contactless conductivity detection ((CD)-D-4) was used for the determination of mono- and disaccharides. CE separation was successfully performed in NaOH solution of the concentration range 25 - 100 mmol/L, pH 12.5 - 12.9. The developed method is characterized by a separation time shorter than 2.5 min. and limit of detection 0.1 mg/L. The method was applied to the determination of saccharides in foods, drinks, and food additives.
引用
收藏
页码:74 / 77
页数:4
相关论文
共 8 条
[1]   Determination of Sugars Using Ligand-Exchange Capillary Electrophoresis [J].
Alekseeva, A. V. ;
Kartsova, L. A. ;
Kazachishcheva, N. V. .
JOURNAL OF ANALYTICAL CHEMISTRY, 2010, 65 (02) :202-208
[2]   Determination of mono- and disaccharides by capillary electrophoresis with contactless conductivity detection [J].
Carvalho, AZ ;
da Silva, JAF ;
do Lago, CL .
ELECTROPHORESIS, 2003, 24 (12-13) :2138-2143
[3]  
Kodicek M., 2007, SACHARIDY BIOCH POJM
[4]   Determination of monosaccharide composition in plant fiber materials by capillary zone electrophoresis [J].
Rovio, Stella ;
Simolin, Helena ;
Koljonen, Krista ;
Siren, Heli .
JOURNAL OF CHROMATOGRAPHY A, 2008, 1185 (01) :139-144
[5]   Determination of neutral carbohydrates by CZE with direct UV detection [J].
Rovio, Stella ;
Yli-Kauhaluoma, Jari ;
Siren, Heli .
ELECTROPHORESIS, 2007, 28 (17) :3129-3135
[6]   Determination of carbohydrates in food samples by capillary electrophoresis with indirect UV detection [J].
Soga, T ;
Serwe, M .
FOOD CHEMISTRY, 2000, 69 (03) :339-344
[7]  
Vodrazka Z, 2002, BIOCHEMIE
[8]   Detection of carbohydrates using new labeling reagent 1-(2-naphthyl)-3-methyl-5-pyrazolone by capillary zone electrophoresis with absorbance (UV) [J].
You, Jinmao ;
Sheng, Xiao ;
Ding, Chenxu ;
Sun, Zhiwei ;
Suo, Yourui ;
Wang, Honglun ;
Li, Win .
ANALYTICA CHIMICA ACTA, 2008, 609 (01) :66-75