Ultrasound promoted expeditious, catalyst-free and solvent-free approach for the synthesis of N,N′-diarylsubstituted formamidines at room temperature

被引:18
|
作者
Dar, Bashir Ahmad [1 ]
Ahmad, Syed Naseer [2 ]
Wagay, Mohammad Arif [1 ]
Hussain, Altaf [1 ]
Ahmad, Nisar [1 ]
Bhat, Khursheed Ahmad [2 ]
Khuroo, Mohammad Akbar [3 ]
Sharma, Meena [4 ]
Singh, Baldev [1 ]
机构
[1] CSIR, Jammu 180001, India
[2] CSIR, Srinagar 190005, Jammu & Kashmir, India
[3] Univ Kashmir, Dept Chem, Srinagar 190006, Jammu & Kashmir, India
[4] Univ Jammu, Dept Chem, Jammu 180004, Jammu & Kashmir, India
关键词
Formamidines; Ultrasonication; Green chemistry; Crystallization; BENZIMIDAZOLES;
D O I
10.1016/j.tetlet.2013.06.131
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
An effortless and efficient protocol was developed for the synthesis of N,N'-diarylsubstituted formamidines under environment-friendly conditions. Ultrasonic energy was employed to obtain the desired products in excellent yields with high purity under solvent-free and catalyst-free conditions. Products were purified by the crystallization technique to avoid excess utilization of organic solvents. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:4880 / 4884
页数:5
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