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Ultrasound promoted expeditious, catalyst-free and solvent-free approach for the synthesis of N,N′-diarylsubstituted formamidines at room temperature
被引:18
|作者:
Dar, Bashir Ahmad
[1
]
Ahmad, Syed Naseer
[2
]
Wagay, Mohammad Arif
[1
]
Hussain, Altaf
[1
]
Ahmad, Nisar
[1
]
Bhat, Khursheed Ahmad
[2
]
Khuroo, Mohammad Akbar
[3
]
Sharma, Meena
[4
]
Singh, Baldev
[1
]
机构:
[1] CSIR, Jammu 180001, India
[2] CSIR, Srinagar 190005, Jammu & Kashmir, India
[3] Univ Kashmir, Dept Chem, Srinagar 190006, Jammu & Kashmir, India
[4] Univ Jammu, Dept Chem, Jammu 180004, Jammu & Kashmir, India
关键词:
Formamidines;
Ultrasonication;
Green chemistry;
Crystallization;
BENZIMIDAZOLES;
D O I:
10.1016/j.tetlet.2013.06.131
中图分类号:
O62 [有机化学];
学科分类号:
070303 ;
081704 ;
摘要:
An effortless and efficient protocol was developed for the synthesis of N,N'-diarylsubstituted formamidines under environment-friendly conditions. Ultrasonic energy was employed to obtain the desired products in excellent yields with high purity under solvent-free and catalyst-free conditions. Products were purified by the crystallization technique to avoid excess utilization of organic solvents. (C) 2013 Elsevier Ltd. All rights reserved.
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页码:4880 / 4884
页数:5
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