Sol-gel processing of ZnS

被引:62
作者
Stanic, V [1 ]
Etsell, TH [1 ]
Pierre, AC [1 ]
Mikula, RJ [1 ]
机构
[1] CANADA CTR MINERAL & ENERGY TECHNOL,WESTERN RES CTR,DEVON,AB T0C 1E0,CANADA
关键词
sol-gel processing; alkoxides; zinc sulfide gel; metal sulfides;
D O I
10.1016/S0167-577X(96)00237-6
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A sol-gel process has been developed for the chemical synthesis of ZnS at room temperature using zinc tert-butoxide and H2S as precursors in a toluene solution. The obtained reaction product was a yellow semi-transparent gel which dried to a reddish-orange solid. Characterization of the dried gel by XRD, IR and EDS confirmed that the product is ZnS with a Zn/5 atomic ratio approximate to 1:1.
引用
收藏
页码:35 / 38
页数:4
相关论文
共 14 条
[1]   MORPHOLOGY OF ZINC-SULFIDE PARTICLES PRODUCED FROM VARIOUS ZINC SALTS BY HOMOGENEOUS PRECIPITATION [J].
CELIKKAYA, A ;
AKINC, M .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1990, 73 (02) :245-250
[2]  
CZEKAJ CL, 1988, INORG CHEM, V27, P3263
[3]  
CZEKAJ CL, 1987, THESIS PENNSYLVANIA
[4]  
GORSTEIN AE, 1990, Patent No. 1574538
[5]  
GUITON TA, 1988, BETTER CERAMICS CH 3, V121, P503
[6]  
HADZL D, 1963, MANUAL DEVICES INFRA, P261
[7]  
Johnson C. E., 1986, Proceedings of the SPIE - The International Society for Optical Engineering, V683, P112, DOI 10.1117/12.936425
[8]   PREPARATION, PURIFICATION, AND DENSIFICATION OF ZINC-SULFIDE POWDER FROM ORGANOMETALLICS [J].
JOHNSON, CE ;
HARRIS, DC ;
WILLINGHAM, CB .
CHEMISTRY OF MATERIALS, 1990, 2 (02) :141-149
[9]  
Klung HP., 1974, XRAY DIFFRACTION PRO, P687
[10]  
POUCHER CJ, 1981, ALDRICH LIB IR SPECT