Headspace solid-phase micro extraction coupled to comprehensive two-dimensional with time-of-flight mass spectrometry applied to the evaluation of Nebbiolo-based wine volatile aroma during ageing

被引:30
作者
Bordiga, Matteo [1 ]
Piana, Gianluca [1 ]
Coisson, Jean Daniel [1 ]
Travaglia, Fabiano [1 ]
Arlorio, Marco [1 ]
机构
[1] Univ Piemonte Orientale, Dipartimento Sci Farmaco, I-28100 Novara, Italy
关键词
GAS CHROMATOGRAPHY-OLFACTOMETRY; OAK WOOD; RED WINES; COMPONENTS; ODORANTS;
D O I
10.1111/ijfs.12366
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
Summary: This study presents the application of a headspace solid-phase microextraction (HS-SPME) method on the analysis of Nebbiolo-based wine volatiles by comprehensive two-dimensional gas chromatography (GC×GC) and time-of-flight mass spectrometry (TOF-MS). The aroma patterns were established for different samples of Nebbiolo-based wines, aged in oak wood barrels for 18 months at constant temperature. The methodology allowed for the simultaneous analysis of over 130 different volatile compounds detected in the headspace. The odour activity values (OAVs) were assessed to identify potentially important odorants of Nebbiolo-based wine during ageing. The highest OAVs were obtained for several compounds such as ethyl octanoate, ethyl hexanoate, isoamyl acetate, β-damascenone, ethyl cinnamate, ethyl 3-methylbutanate and acetaldehyde. Ethyl butanoate, octanoic acid, ethyl dihydrocinnamate and γ-nonalactone were also at concentrations higher than their corresponding threshold. Also vanillin, (E)-whisky lactone, (Z)-whisky lactone, guaiacol and 4-ethyl guaiacol seem to be important odorants after oak wood ageing period. © 2013 Institute of Food Science and Technology.
引用
收藏
页码:787 / 796
页数:10
相关论文
共 30 条
[1]   Yeast influence on volatile composition of wines [J].
Antonelli, A ;
Castellari, L ;
Zambonelli, C ;
Carnacini, A .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (03) :1139-1144
[2]   Hydrolysis of glycosidically bound flavour compounds from oak wood by Oenococcus oeni [J].
Bloem, Audrey ;
Lonvaud-Funel, Aline ;
de Revel, Gilles .
FOOD MICROBIOLOGY, 2008, 25 (01) :99-104
[3]   Aroma compounds of an Italian wine (Ruche) by HS-SPME analysis coupled with GC-ITMS [J].
Bonino, M ;
Schellino, R ;
Rizzi, C ;
Aigotti, R ;
Delfini, C ;
Baiocchi, C .
FOOD CHEMISTRY, 2003, 80 (01) :125-133
[4]   Characterization of Muscat wines aroma evolution using comprehensive gas chromatography followed by a post-analytic approach to 2D contour plots comparison [J].
Bordiga, Matteo ;
Rinaldi, Maurizio ;
Locatelli, Monica ;
Piana, Gianluca ;
Travaglia, Fabiano ;
Coisson, Jean Daniel ;
Arlorio, Marco .
FOOD CHEMISTRY, 2013, 140 (1-2) :57-67
[5]   Chemical and chromatic characteristics of Tempranillo, Cabernet Sauvignon and Merlot wines from DO Navarra aged in Spanish and French oak barrels [J].
Cadahia, Estrella ;
Fernandez de Simon, Brigida ;
Sanz, Miriam ;
Poveda, Pilar ;
Colio, Javier .
FOOD CHEMISTRY, 2009, 115 (02) :639-649
[6]   Volatile composition of aged wine in used barrels of French oak and of American oak [J].
Cerdán, TG ;
Mozaz, SR ;
Azpilicueta, CA .
FOOD RESEARCH INTERNATIONAL, 2002, 35 (07) :603-610
[7]   Monitoring toasting intensity of barrels by chromatographic analysis of volatile compounds from toasted oak wood [J].
Chatonnet, P ;
Cutzach, I ;
Poñs, M ;
Dubourdieu, D .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (10) :4310-4318
[8]   Gas chromatography-olfactometry and chemical quantitative study of the aroma of six premium quality Spanish aged red wines [J].
Culleré, L ;
Escudero, A ;
Cacho, J ;
Ferreira, V .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2004, 52 (06) :1653-1660
[9]   Volatile compounds and sensorial characterization of wines from four Spanish denominations of origin, aged in Spanish Rebollo (Quercus pyrenaica Willd.) oak wood barrels [J].
de Simon, Brigida Fernandez ;
Cadahia, Estrella ;
Sanz, Miriam ;
Poveda, Pilar ;
Perez-Magarino, Silvia ;
Ortega-Heras, Miriam ;
Gonzalez-Huerta, Carlos .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2008, 56 (19) :9046-9055
[10]   Analytical characterization of the aroma of five premium red wines.: Insights into the role of odor families and the concept of fruitiness of wines [J].
Escudero, Ana ;
Campo, Eva ;
Farina, Laura ;
Cacho, Juan ;
Ferreira, Vicente .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2007, 55 (11) :4501-4510